3-iodo-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

Base Information

Chemical Name:3-iodo-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide
CAS No.:1383474-33-6
Molecular Formula:C₂₃H₂₂F₇IN₂O₂
Molecular Weight:618.333
Hs Code.:

Synonyms:3-iodo-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

Suppliers and Price of 3-iodo-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-iodo-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-iodo-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

There total 3 articles about 3-iodo-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.5%

: 1383474-35-8
3-amino-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

: 1383474-33-6
3-iodo-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

Guidance literature:: 3-amino-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 2h;

With urea; In water; for 0.25h;

With potassium iodide; In water; at 20 ℃; for 2h;
DOI:10.1002/cjoc.201100746

Reference yield:

: 107-85-7
1-amino-3-methylbutane

: 1383474-33-6
3-iodo-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / tetrahydrofuran / 20 °C

2.1: palladium 10% on activated carbon; hydrogen / methanol / 60 °C

3.1: hydrogenchloride; sodium nitrite / water / 2 h / 0 °C

3.2: 0.25 h

3.3: 2 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; potassium carbonate; sodium nitrite; In tetrahydrofuran; methanol; water;
DOI:10.1002/cjoc.201100746

Reference yield:

: 494774-76-4
2-(2-methyl-4-(perfluoropropan-2-yl)phenyl)-4-nitro-isoindoline-1,3-dione

: 1383474-33-6
3-iodo-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / tetrahydrofuran / 20 °C

2.1: palladium 10% on activated carbon; hydrogen / methanol / 60 °C

3.1: hydrogenchloride; sodium nitrite / water / 2 h / 0 °C

3.2: 0.25 h

3.3: 2 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; potassium carbonate; sodium nitrite; In tetrahydrofuran; methanol; water;
DOI:10.1002/cjoc.201100746