Technology Process of C23H16ClNO3
There total 7 articles about C23H16ClNO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
10% Pd/C; hydrogen;
In
ethyl acetate;
at 20 ℃;
for 4h;
under 760.051 Torr;
DOI:10.1021/jm301084z
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: dimethyl amine / acetic acid / 3 h / 0 °C / pH 12
2.1: toluene / 12 h
3.1: water; acetonitrile / 5 h / Reflux
4.1: hydrogenchloride; water / 1,4-dioxane / 2 h / Reflux
5.1: caesium carbonate / N,N-dimethyl-formamide / 5 h / 0 - 20 °C
6.1: potassium tert-butylate / tetrahydrofuran / 1 h / -40 °C
6.2: 3 h
7.1: 10% Pd/C; hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr
With
hydrogenchloride; 10% Pd/C; potassium tert-butylate; water; hydrogen; caesium carbonate; dimethyl amine;
In
tetrahydrofuran; 1,4-dioxane; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/jm301084z
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; water / 1,4-dioxane / 2 h / Reflux
2.1: caesium carbonate / N,N-dimethyl-formamide / 5 h / 0 - 20 °C
3.1: potassium tert-butylate / tetrahydrofuran / 1 h / -40 °C
3.2: 3 h
4.1: 10% Pd/C; hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr
With
hydrogenchloride; 10% Pd/C; potassium tert-butylate; water; hydrogen; caesium carbonate;
In
tetrahydrofuran; 1,4-dioxane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm301084z
