1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide

Base Information

Chemical Name:1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide
CAS No.:1620661-24-6
Molecular Formula:C₂₂H₃₉N₂OP
Molecular Weight:378.538
Hs Code.:

Synonyms:1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide

Chemical Property:

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Technology Process of 1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide

There total 5 articles about 1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1620661-20-2
[(di-tert-butylphosphanyl)-4-methoxyphenylamino]diisopropylaminocarbene

: 1620661-24-6
1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide

Guidance literature:: under 0.05 Torr; Heating;
DOI:10.1002/ejic.201402166

Reference yield:

: 1569097-11-5
{[(di-tert-butylphosphanyl)(4-methoxyphenyl)amino]methylene}-diisopropylammonium trifluoromethanesulfonate

: 1620661-24-6
1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -90 - 20 °C

2: 0.05 Torr / Heating

With lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1002/ejic.201402166

Reference yield:

: 1569097-05-7
{[(di-tert-butylphosphoroselenoyl)(4-methoxyphenyl)amino]methylene}diisopropylammonium trifluoromethanesulfonate

: 1620661-24-6
1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide

Guidance literature:: Multi-step reaction with 3 steps

1: Hexamethylphosphorous triamide / dichloromethane / 0.5 h / 20 °C

2: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -90 - 20 °C

3: 0.05 Torr / Heating

With lithium hexamethyldisilazane; Hexamethylphosphorous triamide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejic.201402166