[(di-tert-butylphosphanyl)-4-methoxyphenylamino]diisopropylaminocarbene

Base Information

Chemical Name:[(di-tert-butylphosphanyl)-4-methoxyphenylamino]diisopropylaminocarbene
CAS No.:1620661-20-2
Molecular Formula:C₂₂H₃₉N₂OP
Molecular Weight:378.538
Hs Code.:

Synonyms:[(di-tert-butylphosphanyl)-4-methoxyphenylamino]diisopropylaminocarbene

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Chemical Property of [(di-tert-butylphosphanyl)-4-methoxyphenylamino]diisopropylaminocarbene

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Technology Process of [(di-tert-butylphosphanyl)-4-methoxyphenylamino]diisopropylaminocarbene

There total 3 articles about [(di-tert-butylphosphanyl)-4-methoxyphenylamino]diisopropylaminocarbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1569097-11-5
{[(di-tert-butylphosphanyl)(4-methoxyphenyl)amino]methylene}-diisopropylammonium trifluoromethanesulfonate

: 1620661-20-2
[(di-tert-butylphosphanyl)-4-methoxyphenylamino]diisopropylaminocarbene

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -90 - 20 ℃; for 1h;
DOI:10.1002/ejic.201402166

Reference yield:

: 1569097-01-3
P,P-di-tert-butyl-N-(4-methoxyphenyl)phosphinoselenoic amide

: 1620661-20-2
[(di-tert-butylphosphanyl)-4-methoxyphenylamino]diisopropylaminocarbene

Guidance literature:: Multi-step reaction with 3 steps

1: 3 h / 0 - 20 °C

2: Hexamethylphosphorous triamide / dichloromethane / 0.5 h / 20 °C

3: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -90 - 20 °C

With lithium hexamethyldisilazane; Hexamethylphosphorous triamide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejic.201402166

Reference yield:

: 1569097-05-7
{[(di-tert-butylphosphoroselenoyl)(4-methoxyphenyl)amino]methylene}diisopropylammonium trifluoromethanesulfonate

: 1620661-20-2
[(di-tert-butylphosphanyl)-4-methoxyphenylamino]diisopropylaminocarbene

Guidance literature:: Multi-step reaction with 2 steps

1: Hexamethylphosphorous triamide / dichloromethane / 0.5 h / 20 °C

2: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -90 - 20 °C

With lithium hexamethyldisilazane; Hexamethylphosphorous triamide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejic.201402166