W(C₅(CH₃)5)(NO)(CH₂C₆H₅)(C₆H₅)

Base Information

Chemical Name:W(C₅(CH₃)5)(NO)(CH₂C₆H₅)(C₆H₅)
CAS No.:329769-62-2
Molecular Formula:C₂₃H₂₇NOW
Molecular Weight:517.323
Hs Code.:

W(C<sub>5</sub>(CH<sub>3</sub>)5)(NO)(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)(C<sub>6</sub>H<sub>5</sub>)

Synonyms:W(C₅(CH₃)5)(NO)(CH₂C₆H₅)(C₆H₅)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of W(C₅(CH₃)5)(NO)(CH₂C₆H₅)(C₆H₅)

Chemical Property:

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Technology Process of W(C₅(CH₃)5)(NO)(CH₂C₆H₅)(C₆H₅)

There total 2 articles about W(C₅(CH₃)5)(NO)(CH₂C₆H₅)(C₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 329769-61-1
[(C₅(CH₃)5)W(NO)(CH₂C₆H₅)(CH₂C(CH₃)3)]

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 329769-62-2
W(C₅(CH₃)5)(NO)(CH₂C₆H₅)(C₆H₅)

Guidance literature:: In benzene; byproducts: neopentane; glove box, vac. line or inert atm.; thermolysis of the W complex in benzene at 70°C for 40 h; volatiles removed, residue extd. with Et2O/hexanes (4/1), filtd.; crystn. from filtrate on cooling; elem. anal.;
DOI:10.1021/ja002457e

Reference yield:

: 329769-61-1
[(C₅(CH₃)5)W(NO)(CH₂C₆H₅)(CH₂C(CH₃)3)]

: 1076-43-3
benzene-d6

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 329769-62-2
W(C₅(CH₃)5)(NO)(CH₂C₆H₅)(C₆H₅)

: (C₅(CH₃)5)W(NO)(CH⁽²⁾HC₆H₅)(C₆⁽²⁾H₅)

Guidance literature:: In benzene-d6; benzene; under anaerobic and anhyd. conditions; W complex in benzene-benzene-d6 mixt. stirred and heated at 70°C for 40 h; not isolated; detd. by (1)H NMR spectroscopy; d0 and d6 complexes of W in 1.17:1 ratio obtained;
DOI:10.1021/om010380c