3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

Base Information

Chemical Name:3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide
CAS No.:947530-61-2
Molecular Formula:C₂₀H₂₀BrNO₃
Molecular Weight:402.288
Hs Code.:

Synonyms:3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

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Chemical Property of 3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

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Technology Process of 3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

There total 2 articles about 3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 162330-95-2
β-(2-bromo-4,5-dimethoxyphenyl)-N-methylethylamine

: 1033811-99-2
Phenyl-propynoic acid 2,5-dioxo-pyrrolidin-1-yl ester

: 947530-61-2
3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

Guidance literature:: In 1,4-dioxane; at 20 ℃;
DOI:10.1021/ol071079g

Reference yield:

: 637-44-5
phenylpropyolic acid

: 947530-61-2
3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: DCC / dioxane / 20 °C

2: 100 percent / dioxane / 20 °C

With dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/ol071079g

Reference yield: 68.0%

: 947530-61-2
3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

: 1-benzylidene-7,8-dimethoxy-3-methyl-1,3,4,5-tetrahydrobenzo[d]azepin-2-one

Guidance literature:: With sodium formate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 110 ℃; for 0.25h; microwave irradiation;
DOI:10.1021/ol071079g