3,4-dihydro-3-methyl-2-phenyl-6-trifluoromethylquinoxaline

Base Information

Chemical Name:3,4-dihydro-3-methyl-2-phenyl-6-trifluoromethylquinoxaline
CAS No.:102729-50-0
Molecular Formula:C₁₆H₁₃F₃N₂
Molecular Weight:290.288
Hs Code.:

Synonyms:3,4-dihydro-3-methyl-2-phenyl-6-trifluoromethylquinoxaline

Suppliers and Price of 3,4-dihydro-3-methyl-2-phenyl-6-trifluoromethylquinoxaline

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Chemical Property of 3,4-dihydro-3-methyl-2-phenyl-6-trifluoromethylquinoxaline

Chemical Property:

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Technology Process of 3,4-dihydro-3-methyl-2-phenyl-6-trifluoromethylquinoxaline

There total 11 articles about 3,4-dihydro-3-methyl-2-phenyl-6-trifluoromethylquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 368-71-8
4-(trifluoromethyl)-1,2-phenylenediamine

: 102729-50-0
3,4-dihydro-3-methyl-2-phenyl-6-trifluoromethylquinoxaline

Guidance literature:: Multi-step reaction with 5 steps

1: 18 percent / ethanol / 3 h / Heating

2: 84 percent / POCl₃ / 2 h / Heating

3: 77 percent / H₂, NEt₃ / 10percent Pd/C / ethanol / 1 h / 18 °C / 2280 Torr

4: 81 percent / 30percent H₂O₂, conc. HCl / methanol / 0.5 h / Ambient temperature

5: diethyl ether / 24 h

With hydrogenchloride; hydrogen; dihydrogen peroxide; triethylamine; trichlorophosphate; palladium on activated charcoal; In methanol; diethyl ether; ethanol;

Reference yield:

: 121-17-5
2-chloro-3-nitro-5-trifluoromethylbenzene

: 102729-50-0
3,4-dihydro-3-methyl-2-phenyl-6-trifluoromethylquinoxaline

Guidance literature:: Multi-step reaction with 7 steps

1: 87 percent Turnov_. / NaHCO₃ / ethanol; H₂O / 24 h / Heating

2: 57 percent / H₂ / 10percent Pd/C / ethanol / 1 h / 18 °C / 740 Torr

3: 70 percent / 10percent NaOH, 30percent H₂O₂ / 1 h / 100 °C

4: 84 percent / POCl₃ / 2 h / Heating

5: 77 percent / H₂, NEt₃ / 10percent Pd/C / ethanol / 1 h / 18 °C / 2280 Torr

6: 81 percent / 30percent H₂O₂, conc. HCl / methanol / 0.5 h / Ambient temperature

7: diethyl ether / 24 h

With hydrogenchloride; sodium hydroxide; hydrogen; dihydrogen peroxide; sodium hydrogencarbonate; triethylamine; trichlorophosphate; palladium on activated charcoal; In methanol; diethyl ether; ethanol; water;

Reference yield:

: 611-73-4
Benzoylformic acid

: 102729-50-0
3,4-dihydro-3-methyl-2-phenyl-6-trifluoromethylquinoxaline

Guidance literature:: Multi-step reaction with 5 steps

1: 18 percent / ethanol / 3 h / Heating

2: 84 percent / POCl₃ / 2 h / Heating

3: 77 percent / H₂, NEt₃ / 10percent Pd/C / ethanol / 1 h / 18 °C / 2280 Torr

4: 81 percent / 30percent H₂O₂, conc. HCl / methanol / 0.5 h / Ambient temperature

5: diethyl ether / 24 h

With hydrogenchloride; hydrogen; dihydrogen peroxide; triethylamine; trichlorophosphate; palladium on activated charcoal; In methanol; diethyl ether; ethanol;