2-DEOXY-ALPHA-D-RIBOSE 1-PHOSPHATE DI(MONOCYCLOHEXYL-AMMONIUM) SALT

Base Information

• Chemical Name: 2-DEOXY-ALPHA-D-RIBOSE 1-PHOSPHATE DI(MONOCYCLOHEXYL-AMMONIUM) SALT
• CAS No.: 102783-28-8
• Molecular Formula: C₅H₁₁O₇P*2C₆H₁₃N
• Molecular Weight: 412.464
• Mol file: 102783-28-8.mol

Synonyms:2-DEOXY-ALPHA-D-RIBOSE 1-PHOSPHATE BIS(CYCLOHEXYLAMINE) SALT;2-DEOXY-ALPHA-D-RIBOSE 1-PHOSPHATE DI(MONOCYCLOHEXYL-AMMONIUM) SALT;2-DEOXY-A-D-RIBOSE 1-PHOSPHATE*DI(MONOCY CLOHEXYLAMM;2-DEOXY-ALPHA-D-RIBOSE1-PHOSPHATE BIS &;2-deoxy-α-d-ribose 1-phosphate bis(cyclohexylammonium) salt;2-Deoxy-α-D-ribose1-phosphatebis(cyclohexylamine)salt;2-Deoxy-á-D-ribose-1-phosphate di(monocyclohexylammonium) salt;2-deoxy-alpha-D-ribose-1-phosphate bis(cyclohexylamine)

Chemical Property of 2-DEOXY-ALPHA-D-RIBOSE 1-PHOSPHATE DI(MONOCYCLOHEXYL-AMMONIUM) SALT

Chemical Property:

• Melting Point: 168 - 169 °C (diethyl ether)
• PSA: 178.30000
• LogP: 2.52010
• Storage Temp.: −20°C
• Solubility.: H2O: 50 mg/mL, clear, faintly yellow

Purity/Quality:

98%min ^*data from raw suppliers

2-Deoxy-α-D-ribose 1-phosphate bis(cyclohexylammonium) salt ≥97% ^*data from reagent suppliers

Safty Information:

• Safety Statements: 22-24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-DEOXY-ALPHA-D-RIBOSE 1-PHOSPHATE DI(MONOCYCLOHEXYL-AMMONIUM) SALT

There total 5 articles about 2-DEOXY-ALPHA-D-RIBOSE 1-PHOSPHATE DI(MONOCYCLOHEXYL-AMMONIUM) SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

bis(cyclohexylamine) 3',5'-O-bis(4-chlorobenzoyl)-2-deoxy-α-D-ribosyl-1-phosphate → α-D-2′-deoxyribofuranose-1-O-phosphate bis(cyclohexylammonium) salt (98693-55-1,102783-28-8)

Guidance literature:

With cyclohexylamine; In methanol; at 20 ℃; for 72h;

DOI:10.1021/jo025793h

Reference yield: 74.0%

bis(cyclohexylammonium) phosphate (37832-40-9,36011-98-0) + 7-methyl-2′-deoxyguanosine hydroiodide → α-D-2′-deoxyribofuranose-1-O-phosphate bis(cyclohexylammonium) salt (98693-55-1,102783-28-8)

Guidance literature:

With purine nucleoside phosphorylase; In water; at 20 ℃; for 5h; Enzymatic reaction;

DOI:10.1002/ejoc.201901454

Reference yield:

cyclohexylamine (108-91-8,157973-60-9) → α-D-2′-deoxyribofuranose-1-O-phosphate bis(cyclohexylammonium) salt (98693-55-1,102783-28-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 13.5 g / various solvent(s) / 2 h / 0 °C

2: 85 percent / cyclohexylamine / methanol / 72 h / 20 °C

With cyclohexylamine; In methanol;

DOI:10.1021/jo025793h

upstream raw materials:

cyclohexylamine

3,5-O-bis(4-chlorobenzoyl)-2-deoxy-α-D-ribofuranosyl chloride

bis(cyclohexylammonium) phosphate

Downstream raw materials:

2-chloro-2'-deoxyadenosine

2-thiodeoxycytidine

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