9-(3-O-benzoyl-6-deoxy-β-D-glycero-hex-2-enopyranosyl-4-ulose)hypoxanthine

Base Information

Chemical Name:9-(3-O-benzoyl-6-deoxy-β-D-glycero-hex-2-enopyranosyl-4-ulose)hypoxanthine
CAS No.:103365-24-8
Molecular Formula:C₁₈H₁₄N₄O₅
Molecular Weight:366.333
Hs Code.:

Synonyms:9-(3-O-benzoyl-6-deoxy-β-D-glycero-hex-2-enopyranosyl-4-ulose)hypoxanthine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(3-O-benzoyl-6-deoxy-β-D-glycero-hex-2-enopyranosyl-4-ulose)hypoxanthine

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Technology Process of 9-(3-O-benzoyl-6-deoxy-β-D-glycero-hex-2-enopyranosyl-4-ulose)hypoxanthine

There total 7 articles about 9-(3-O-benzoyl-6-deoxy-β-D-glycero-hex-2-enopyranosyl-4-ulose)hypoxanthine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 108-24-7
acetic anhydride

: 103285-88-7
9-(2,3-di-O-benzoyl-6-deoxy-β-D-glucopyranosyl)hypoxanthine

: 103365-24-8
9-(3-O-benzoyl-6-deoxy-β-D-glycero-hex-2-enopyranosyl-4-ulose)hypoxanthine

Guidance literature:: In dimethyl sulfoxide; at 100 ℃; for 0.166667h;
DOI:10.1016/0008-6215(86)80048-9

Reference yield:

: 98-88-4
benzoyl chloride

: 103365-24-8
9-(3-O-benzoyl-6-deoxy-β-D-glycero-hex-2-enopyranosyl-4-ulose)hypoxanthine

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / pyridine / 8 h / -20 °C

2: 65 percent / sodium nitrite, acetic acid / H₂O / 6 h / Ambient temperature

3: 65 percent / dimethylsulfoxide / 0.17 h / 100 °C

With pyridine; acetic acid; sodium nitrite; In water; dimethyl sulfoxide;
DOI:10.1016/0008-6215(86)80048-9

Reference yield:

: 103365-23-7
9-(6-deoxy-β-D-glucopyranosyl)adenine

: 103365-24-8
9-(3-O-benzoyl-6-deoxy-β-D-glycero-hex-2-enopyranosyl-4-ulose)hypoxanthine

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / pyridine / 8 h / -20 °C

2: 65 percent / sodium nitrite, acetic acid / H₂O / 6 h / Ambient temperature

3: 65 percent / dimethylsulfoxide / 0.17 h / 100 °C

With pyridine; acetic acid; sodium nitrite; In water; dimethyl sulfoxide;
DOI:10.1016/0008-6215(86)80048-9