Allyl 6β-<(2R)-2-(4-Ethyl-2,3-dioxopiperazin-1-ylcarbonylamino)-2-phenylacetamido>-6α-succinimidopenicillanate

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Chemical Name:Allyl 6β-<(2R)-2-(4-Ethyl-2,3-dioxopiperazin-1-ylcarbonylamino)-2-phenylacetamido>-6α-succinimidopenicillanate
CAS No.:137839-99-7
Molecular Formula:C₃₀H₃₄N₆O₁₀S
Molecular Weight:670.7
Hs Code.:

Synonyms:Allyl 6β-<(2R)-2-(4-Ethyl-2,3-dioxopiperazin-1-ylcarbonylamino)-2-phenylacetamido>-6α-succinimidopenicillanate

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Chemical Property of Allyl 6β-<(2R)-2-(4-Ethyl-2,3-dioxopiperazin-1-ylcarbonylamino)-2-phenylacetamido>-6α-succinimidopenicillanate

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Technology Process of Allyl 6β-<(2R)-2-(4-Ethyl-2,3-dioxopiperazin-1-ylcarbonylamino)-2-phenylacetamido>-6α-succinimidopenicillanate

There total 7 articles about Allyl 6β-<(2R)-2-(4-Ethyl-2,3-dioxopiperazin-1-ylcarbonylamino)-2-phenylacetamido>-6α-succinimidopenicillanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 137839-98-6
Allyl 6β-<(2R)-2-(4-Ethyl-2,3-dioxopiperazin-1-ylcarbonylamino)-2-phenylacetamido>-6α-methylthiopenicillanate

: 137839-99-7
Allyl 6β-<(2R)-2-(4-Ethyl-2,3-dioxopiperazin-1-ylcarbonylamino)-2-phenylacetamido>-6α-succinimidopenicillanate

Guidance literature:: silver(I) acetate; In N,N-dimethyl-formamide; for 1h; Ambient temperature;

Reference yield:

: 63422-71-9
(R)-α-[[(4-ethyl-2,3-dioxo-1-piperazinyl)carbonyl]amino]benzeneacetic acid

: 137839-99-7
Allyl 6β-<(2R)-2-(4-Ethyl-2,3-dioxopiperazin-1-ylcarbonylamino)-2-phenylacetamido>-6α-succinimidopenicillanate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride, DMF / CH₂Cl₂ / 1 h / Ambient temperature

2: 45 percent / pyridine / CH₂Cl₂ / 2 h / Ambient temperature

3: 44 percent / AgOAc / dimethylformamide / 1 h / Ambient temperature

With pyridine; oxalyl dichloride; N,N-dimethyl-formamide; silver(I) acetate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 87106-48-7
Toluene-p-sulphonate of Allyl 6β-Aminopenicillanate

: 137839-99-7
Allyl 6β-<(2R)-2-(4-Ethyl-2,3-dioxopiperazin-1-ylcarbonylamino)-2-phenylacetamido>-6α-succinimidopenicillanate

Guidance literature:: Multi-step reaction with 5 steps

2: K₂CO₃ / dimethylformamide / 0 deg C, 1.5 h, rt, 1h

3: 2,4-dinitrophenylhydrazine, p-TsOH / ethanol; CHCl₃ / 1 h / Ambient temperature

4: 45 percent / pyridine / CH₂Cl₂ / 2 h / Ambient temperature

5: 44 percent / AgOAc / dimethylformamide / 1 h / Ambient temperature

With pyridine; potassium carbonate; toluene-4-sulfonic acid; (2,4-dinitro-phenyl)-hydrazine; silver(I) acetate; In ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide;