6-benzyloxy-7-methoxy-2-(3-methoxybenzyl)-1-phenyl-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:6-benzyloxy-7-methoxy-2-(3-methoxybenzyl)-1-phenyl-1,2,3,4-tetrahydroisoquinoline
CAS No.:1602589-58-1
Molecular Formula:C₃₁H₃₁NO₃
Molecular Weight:465.592
Hs Code.:

Synonyms:6-benzyloxy-7-methoxy-2-(3-methoxybenzyl)-1-phenyl-1,2,3,4-tetrahydroisoquinoline

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Chemical Property of 6-benzyloxy-7-methoxy-2-(3-methoxybenzyl)-1-phenyl-1,2,3,4-tetrahydroisoquinoline

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Technology Process of 6-benzyloxy-7-methoxy-2-(3-methoxybenzyl)-1-phenyl-1,2,3,4-tetrahydroisoquinoline

There total 5 articles about 6-benzyloxy-7-methoxy-2-(3-methoxybenzyl)-1-phenyl-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 55507-08-9
6-benzyloxy-7-methoxy-1-phenyl-1,2,3,4-tetrahydroisoquinoline

: 824-98-6
m-methoxybenzyl chloride

: 1602589-58-1
6-benzyloxy-7-methoxy-2-(3-methoxybenzyl)-1-phenyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With triethylamine; In ethanol; at 130 ℃; for 1h; Microwave irradiation;
DOI:10.1002/cmdc.201300412

Reference yield:

: 36455-21-7
3-benzyloxy-4-methoxyphenylethylamine

: 1602589-58-1
6-benzyloxy-7-methoxy-2-(3-methoxybenzyl)-1-phenyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / ethanol / 0.5 h / 170 °C / Microwave irradiation

2: trichlorophosphate / toluene / 4 h / 140 °C

3: triethylamine / ethanol / 1 h / 130 °C / Microwave irradiation

With triethylamine; trichlorophosphate; In ethanol; toluene;
DOI:10.1002/cmdc.201300412

Reference yield:

: 98-88-4
benzoyl chloride

: 1602589-58-1
6-benzyloxy-7-methoxy-2-(3-methoxybenzyl)-1-phenyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / ethanol / 0.5 h / 170 °C / Microwave irradiation

2: trichlorophosphate / toluene / 4 h / 140 °C

3: triethylamine / ethanol / 1 h / 130 °C / Microwave irradiation

With triethylamine; trichlorophosphate; In ethanol; toluene;
DOI:10.1002/cmdc.201300412