(((CH₃)3C)2C₆H₃)3C₂₇H₁₁N₄OPd

Base Information

• Chemical Name: (((CH₃)3C)2C₆H₃)3C₂₇H₁₁N₄OPd
• CAS No.: 437653-60-6
• Molecular Formula: C₆₉H₇₄N₄OPd
• Molecular Weight: 1081.79
• Mol file: 437653-60-6.mol

Synonyms:(((CH₃)3C)2C₆H₃)3C₂₇H₁₁N₄OPd

Chemical Property of (((CH₃)3C)2C₆H₃)3C₂₇H₁₁N₄OPd

Chemical Property:

Purity/Quality:

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Technology Process of (((CH₃)3C)2C₆H₃)3C₂₇H₁₁N₄OPd

There total 1 articles about (((CH₃)3C)2C₆H₃)3C₂₇H₁₁N₄OPd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(((CH3)3C)2C6H3)3C27H13N4O + palladium diacetate (3375-31-3) → (((CH3)3C)2C6H3)3C27H11N4OPd (437653-60-6)

Guidance literature:

In toluene; Pd compd. (2.4 equiv.) added to soln. of porphyrin in toluene; heated under reflux for 6 h; evapd.; crystd. (CH2Cl2-MeOH);

DOI:10.1021/ja017531n

Reference yield: 77.0%

4-amino-1,2,4-triazole (584-13-4) + (((CH3)3C)2C6H3)3C27H11N4OPd (437653-60-6) + water (7732-18-5) → (((CH3)3C)2C6H3)3(NH2)C27H10N4OPd*H2O

Guidance literature:

With NaOH; In ethanol; toluene; EtOH, 4-amino-4H-1,2,4-triazole (11.7 equiv.) and NaOH added to toluene soln. of Pd complex; refluxed for 1 h; cooled; washed with water; dried (Na2SO4); filtered (silica gel, CH2Cl2); crystd. (CH2Cl2-MeOH); elem. anal.;

DOI:10.1021/ja017531n

upstream raw materials:

palladium diacetate