(E)-4-pentachlorophenyl 5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>-5-octenoate

Base Information

Chemical Name:(E)-4-pentachlorophenyl 5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>-5-octenoate
CAS No.:120743-59-1
Molecular Formula:C₃₈H₄₉Cl₅O₄Si₂
Molecular Weight:803.241
Hs Code.:

Synonyms:(E)-4-pentachlorophenyl 5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>-5-octenoate

Suppliers and Price of (E)-4-pentachlorophenyl 5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>-5-octenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-pentachlorophenyl 5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>-5-octenoate

Chemical Property:

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Technology Process of (E)-4-pentachlorophenyl 5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>-5-octenoate

There total 5 articles about (E)-4-pentachlorophenyl 5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>-5-octenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 120743-59-1
(E)-4-pentachlorophenyl 5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>-5-octenoate

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 1 h

2: methanol / dimethylformamide

3: DCCI / tetrahydrofuran / 1 h

With 1H-imidazole; methanol; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00127a022

Reference yield:

: 67566-95-4
5,6-bis(4-methoxyphenyl)-5-octenoic acid

: 120743-59-1
(E)-4-pentachlorophenyl 5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>-5-octenoate

Guidance literature:: Multi-step reaction with 4 steps

1: KOH / ethane-1,2-diol / 48 h / 200 °C

2: imidazole / dimethylformamide / 1 h

3: methanol / dimethylformamide

4: DCCI / tetrahydrofuran / 1 h

With 1H-imidazole; methanol; potassium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethylene glycol; N,N-dimethyl-formamide;
DOI:10.1021/jm00127a022

Reference yield:

: 67566-96-5
5,6-bis(4-hydroxyphenyl)-5-octenoic acid

: 120743-59-1
(E)-4-pentachlorophenyl 5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>-5-octenoate

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 1 h

2: methanol / dimethylformamide

3: DCCI / tetrahydrofuran / 1 h

With 1H-imidazole; methanol; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00127a022