1-TRIMETHYLSTANNYL-3,3-DIMETHOXYPROPANE

Base Information

• Chemical Name: 1-TRIMETHYLSTANNYL-3,3-DIMETHOXYPROPANE
• CAS No.: 102402-80-2
• Molecular Formula: C₈H₂₀O₂Sn
• Molecular Weight: 266.956
• Mol file: 102402-80-2.mol

Synonyms:3,3-Dimethoxy-1-(trimethylstannyl)propane

Chemical Property of 1-TRIMETHYLSTANNYL-3,3-DIMETHOXYPROPANE

Chemical Property:

• Boiling Point: 65-75 °C(Press: 1 Torr)
• PSA: 18.46000
• LogP: 2.33360

Purity/Quality:

98%min ^*data from raw suppliers

1-TRIMETHYLSTANNYL-3,3-DIMETHOXYPROPANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-TRIMETHYLSTANNYL-3,3-DIMETHOXYPROPANE

There total 1 articles about 1-TRIMETHYLSTANNYL-3,3-DIMETHOXYPROPANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

3-bromopropanal dimethyl acetal (36255-44-4) + trimethyltin(IV)chloride (1066-45-1) → 1,1-dimethoxy-3-trimethylstannyl propane (102402-80-2)

Guidance literature:

With magnesium; Product distribution;

DOI:10.1016/S0040-4039(00)89209-6

Reference yield:

(Cyclohexa-1,3-dienyloxy)-triphenyl-silane (116760-57-7) + 1,1-dimethoxy-3-trimethylstannyl propane (102402-80-2) → 4-(1-Methoxy-allyl)-cyclohexanone (116760-54-4)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; titanium tetrachloride; Yield given. Multistep reaction;

DOI:10.1016/S0040-4039(00)80184-7

Reference yield:

1,1-dimethoxy-3-trimethylstannyl propane (102402-80-2) + C26H20O7 (125629-59-6) → C30H28O8 (125629-60-9,125711-93-5)

Guidance literature:

With aluminium trichloride; trimethylsilyl trifluoromethanesulfonate; Yield given. Multistep reaction;

DOI:10.1016/S0040-4039(00)99438-3

upstream raw materials:

3-bromopropanal dimethyl acetal

trimethyltin(IV)chloride

Downstream raw materials:

4-(1-Methoxy-allyl)-cyclohexanone

C₃₀H₂₈O₈

Refernces