(2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide trifluoroacetic acid salt

Base Information

Chemical Name:(2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide trifluoroacetic acid salt
CAS No.:1173158-48-9
Molecular Formula:C₂HF₃O₂*C₂₁H₃₅N₃O₄
Molecular Weight:507.551
Hs Code.:

Synonyms:(2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide trifluoroacetic acid salt

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Chemical Property of (2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide trifluoroacetic acid salt

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Technology Process of (2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide trifluoroacetic acid salt

There total 5 articles about (2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1173158-49-0
C₂₅H₃₉N₃O₆

: 76-05-1
trifluoroacetic acid

: 1173158-48-9
(2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide trifluoroacetic acid salt

Guidance literature:: C₂₅H₃₉N₃O₆; With diethylamine; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; In water; acetonitrile; at 22 ℃; for 1h;

trifluoroacetic acid; In water; acetonitrile;

Reference yield:

: 1173157-89-5
6-(prop-2-enyl-butyloxycarbonyl-amino)hexylmethyl sulfonate

: 1173158-48-9
(2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / diethyl ether / 0 - 22 °C

2.1: hydrogenchloride / diethyl ether / 5 h / 22 °C

3.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.25 h / 22 °C

3.2: 1 h

4.1: diethylamine / trisodium tris(3-sulfophenyl)phosphine; palladium diacetate / acetonitrile; water / 1 h / 22 °C

With hydrogenchloride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; diethylamine; N-ethyl-N,N-diisopropylamine; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; In diethyl ether; dichloromethane; water; acetonitrile;

Reference yield:

: 184537-64-2
N-[6-(aminooxy)hexyl]prop-2-enyloxycarboxamide hydrochloric acid salt

: 1173158-48-9
(2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.25 h / 22 °C

1.2: 1 h

2.1: diethylamine / trisodium tris(3-sulfophenyl)phosphine; palladium diacetate / acetonitrile; water / 1 h / 22 °C

With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; diethylamine; N-ethyl-N,N-diisopropylamine; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; In dichloromethane; water; acetonitrile;