6-(Allyloxycarbonylamino)-1-hexanol

Base Information

Chemical Name:6-(Allyloxycarbonylamino)-1-hexanol
CAS No.:146292-92-4
Molecular Formula:C₁₀H₁₉NO₃
Molecular Weight:201.266
Hs Code.:2924199090
European Community (EC) Number:622-820-3
DSSTox Substance ID:DTXSID00408729
Wikidata:Q82214311
Mol file:146292-92-4.mol

Synonyms:6-(Allyloxycarbonylamino)-1-hexanol;146292-92-4;Prop-2-enyl N-(6-hydroxyhexyl)carbamate;PROP-2-EN-1-YL N-(6-HYDROXYHEXYL)CARBAMATE;Allyl N-(6-hydroxyhexyl)carbamate;N-(6-hydroxyhexyl)prop-2-enyloxycarboxamide;SCHEMBL991007;Carbamic acid, (6-hydroxyhexyl)-, 2-propenyl ester;DTXSID00408729;FQFRACFUQCJOMP-UHFFFAOYSA-N;AKOS024386361;MS-21684;A1-18782;J-008207;6-(Allyloxycarbonylamino)-1-hexanol, >=98.0% (GC)

Suppliers and Price of 6-(Allyloxycarbonylamino)-1-hexanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
6-(Allyloxycarbonylamino)-1-hexanol ≥98.0% (GC)
1g
$ 66.80

American Custom Chemicals Corporation
6-(ALLYLOXYCARBONYLAMINO)-1-HEXANOL 95.00%
1G
$ 683.87

AK Scientific
6-(Allyloxycarbonylamino)-1-hexanol
2.5g
$ 2277.00

A1 Biochem Labs
6-(Allyloxycarbonylamino)-1-hexanol 95%
2.5 g
$ 1000.00

Total 2 raw suppliers

Chemical Property of 6-(Allyloxycarbonylamino)-1-hexanol

Chemical Property:

Vapor Pressure:1.37E-05mmHg at 25°C
Melting Point:46-49 °C
Refractive Index:1.466
Boiling Point:328.8°C at 760 mmHg
Flash Point:152.7°C
PSA：58.56000
Density:1.013g/cm³
LogP:1.84220
XLogP3:1.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:9
Exact Mass:201.13649347
Heavy Atom Count:14
Complexity:159

Purity/Quality:

98%Min ^*data from raw suppliers

6-(Allyloxycarbonylamino)-1-hexanol ≥98.0% (GC) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCOC(=O)NCCCCCCO

Technology Process of 6-(Allyloxycarbonylamino)-1-hexanol

There total 1 articles about 6-(Allyloxycarbonylamino)-1-hexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 4048-33-3
6-amino-1-hexanol

: 2937-50-0
Allyl chloroformate

: 146292-92-4
N-(6-hydroxy-hexyl)prop-2-enyloxycarboxamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c4ob00541d

Reference yield:

: 146292-92-4
N-(6-hydroxy-hexyl)prop-2-enyloxycarboxamide

: 1173158-23-0
C₅₀H₉₂N₆O₁₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 0 °C

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / diethyl ether / 0 - 22 °C

3.1: hydrogenchloride / diethyl ether / 5 h / 22 °C

4.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.25 h / 22 °C

4.2: 1 h

5.1: diethylamine / trisodium tris(3-sulfophenyl)phosphine; palladium diacetate / acetonitrile; water / 1 h / 22 °C

6.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h / 22 °C

With hydrogenchloride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; diethylamine; triethylamine; N-ethyl-N,N-diisopropylamine; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 146292-92-4
N-(6-hydroxy-hexyl)prop-2-enyloxycarboxamide

: 1173158-50-3
C₅₁H₈₈N₆O₁₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 0 °C

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / diethyl ether / 0 - 22 °C

3.1: hydrogenchloride / diethyl ether / 5 h / 22 °C

4.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.25 h / 22 °C

4.2: 1 h

5.1: diethylamine / trisodium tris(3-sulfophenyl)phosphine; palladium diacetate / acetonitrile; water / 1 h / 22 °C

6.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h / 22 °C

With hydrogenchloride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; diethylamine; triethylamine; N-ethyl-N,N-diisopropylamine; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;