(2R,3R,5R)-5-((3Z,6Z)-8-(tert-butyldimethylsilyloxy)-3-chloro-10-ethoxy-7-methyl-10-oxodeca-3,6-dienyl)-2-((4-methoxybenzyloxy)methyl)tetrahydrofuran-3-yl benzoate

Base Information

Chemical Name:(2R,3R,5R)-5-((3Z,6Z)-8-(tert-butyldimethylsilyloxy)-3-chloro-10-ethoxy-7-methyl-10-oxodeca-3,6-dienyl)-2-((4-methoxybenzyloxy)methyl)tetrahydrofuran-3-yl benzoate
CAS No.:1041436-98-9
Molecular Formula:C₃₉H₅₅ClO₈Si
Molecular Weight:715.399
Hs Code.:

(2R,3R,5R)-5-((3Z,6Z)-8-(tert-butyldimethylsilyloxy)-3-chloro-10-ethoxy-7-methyl-10-oxodeca-3,6-dienyl)-2-((4-methoxybenzyloxy)methyl)tetrahydrofuran-3-yl benzoate

Synonyms:(2R,3R,5R)-5-((3Z,6Z)-8-(tert-butyldimethylsilyloxy)-3-chloro-10-ethoxy-7-methyl-10-oxodeca-3,6-dienyl)-2-((4-methoxybenzyloxy)methyl)tetrahydrofuran-3-yl benzoate

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Chemical Property of (2R,3R,5R)-5-((3Z,6Z)-8-(tert-butyldimethylsilyloxy)-3-chloro-10-ethoxy-7-methyl-10-oxodeca-3,6-dienyl)-2-((4-methoxybenzyloxy)methyl)tetrahydrofuran-3-yl benzoate

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Technology Process of (2R,3R,5R)-5-((3Z,6Z)-8-(tert-butyldimethylsilyloxy)-3-chloro-10-ethoxy-7-methyl-10-oxodeca-3,6-dienyl)-2-((4-methoxybenzyloxy)methyl)tetrahydrofuran-3-yl benzoate

There total 1 articles about (2R,3R,5R)-5-((3Z,6Z)-8-(tert-butyldimethylsilyloxy)-3-chloro-10-ethoxy-7-methyl-10-oxodeca-3,6-dienyl)-2-((4-methoxybenzyloxy)methyl)tetrahydrofuran-3-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1041436-86-5
ethyl (Z)-3-(tert-butyldimethylsilyloxy)-8,8-dichloro-4-methylocta-4,7-dienoate

: 1041436-82-1
(2R,3R,5S)-2-((4-methoxybenzyloxy)methyl)-5-vinyltetrahydrofuran-3-yl benzoate

: 1041436-98-9
(2R,3R,5R)-5-((3Z,6Z)-8-(tert-butyldimethylsilyloxy)-3-chloro-10-ethoxy-7-methyl-10-oxodeca-3,6-dienyl)-2-((4-methoxybenzyloxy)methyl)tetrahydrofuran-3-yl benzoate

Guidance literature:: (2R,3R,5S)-2-((4-methoxybenzyloxy)methyl)-5-vinyltetrahydrofuran-3-yl benzoate; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 20 ℃; for 5h;

ethyl (Z)-3-(tert-butyldimethylsilyloxy)-8,8-dichloro-4-methylocta-4,7-dienoate; With potassium phosphate; bis[2-(diphenylphosphino)phenyl] ether; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; for 72h; Further stages.; Heating;
DOI:10.1002/anie.200800585