N-[1-(3-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-3-(toluene-4-sulfonylamino)-propionamide; hydriodide

Base Information

Chemical Name:N-[1-(3-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-3-(toluene-4-sulfonylamino)-propionamide; hydriodide
CAS No.:84792-62-1
Molecular Formula:C₂₅H₃₃N₅O₄S*HI
Molecular Weight:627.547
Hs Code.:

Synonyms:N-[1-(3-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-3-(toluene-4-sulfonylamino)-propionamide; hydriodide

Suppliers and Price of N-[1-(3-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-3-(toluene-4-sulfonylamino)-propionamide; hydriodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[1-(3-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-3-(toluene-4-sulfonylamino)-propionamide; hydriodide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[1-(3-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-3-(toluene-4-sulfonylamino)-propionamide; hydriodide

There total 7 articles about N-[1-(3-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-3-(toluene-4-sulfonylamino)-propionamide; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 93235-80-4
3-{3-Oxo-3-piperidin-1-yl-2-[3-(toluene-4-sulfonylamino)-propionylamino]-propyl}-thiobenzimidic acid methyl ester; hydriodide

: 84792-62-1
N-[1-(3-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-3-(toluene-4-sulfonylamino)-propionamide; hydriodide

Guidance literature:: With ammonium acetate; In ethanol; at 60 ℃; for 2.5h;

Reference yield:

: 42908-33-8
3-{[(4-methylphenyl)sulfonyl]amino}propanoic acid

: 84792-62-1
N-[1-(3-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-3-(toluene-4-sulfonylamino)-propionamide; hydriodide

Guidance literature:: Multi-step reaction with 7 steps

1: SOCl₂ / 1 h / Heating

2: 50 percent / NaOH (1 mol/l) / diethyl ether; H₂O / 6 h / Ambient temperature

3: 35 percent / DCC / pyridine / 24 h

4: 67 percent / pyridine / 24 h / Ambient temperature

5: 62 percent / TEA, H₂S / pyridine / 48 h / Ambient temperature

6: 42 percent / ethanol / 0.25 h / 70 °C

7: 77 percent / CH₃COONH₄ / ethanol / 2.5 h / 60 °C

With sodium hydroxide; thionyl chloride; TEA; hydrogen sulfide; ammonium acetate; dicyclohexyl-carbodiimide; In pyridine; diethyl ether; ethanol; water;

Reference yield:

: 61341-03-5
N-(toluene-4-sulfonyl)-β-alanyl chloride

: 84792-62-1
N-[1-(3-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-3-(toluene-4-sulfonylamino)-propionamide; hydriodide

Guidance literature:: Multi-step reaction with 6 steps

1: 50 percent / NaOH (1 mol/l) / diethyl ether; H₂O / 6 h / Ambient temperature

2: 35 percent / DCC / pyridine / 24 h

3: 67 percent / pyridine / 24 h / Ambient temperature

4: 62 percent / TEA, H₂S / pyridine / 48 h / Ambient temperature

5: 42 percent / ethanol / 0.25 h / 70 °C

6: 77 percent / CH₃COONH₄ / ethanol / 2.5 h / 60 °C

With sodium hydroxide; TEA; hydrogen sulfide; ammonium acetate; dicyclohexyl-carbodiimide; In pyridine; diethyl ether; ethanol; water;