(9aS)-8-acetyl-N-{4-[(2,4-dichlorobenzyl)oxy]-2,3,6-trimethylbenzyl}-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide

Base Information

Chemical Name:(9aS)-8-acetyl-N-{4-[(2,4-dichlorobenzyl)oxy]-2,3,6-trimethylbenzyl}-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide
CAS No.:925440-72-8
Molecular Formula:C₃₄H₃₁Cl₂NO₈
Molecular Weight:652.528
Hs Code.:

(9aS)-8-acetyl-N-{4-[(2,4-dichlorobenzyl)oxy]-2,3,6-trimethylbenzyl}-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide

Synonyms:(9aS)-8-acetyl-N-{4-[(2,4-dichlorobenzyl)oxy]-2,3,6-trimethylbenzyl}-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide

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Chemical Property of (9aS)-8-acetyl-N-{4-[(2,4-dichlorobenzyl)oxy]-2,3,6-trimethylbenzyl}-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide

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Technology Process of (9aS)-8-acetyl-N-{4-[(2,4-dichlorobenzyl)oxy]-2,3,6-trimethylbenzyl}-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide

There total 2 articles about (9aS)-8-acetyl-N-{4-[(2,4-dichlorobenzyl)oxy]-2,3,6-trimethylbenzyl}-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 925440-61-5
(9aS)-8-Acetyl-1,7-dihydroxy-N-(4-hydroxy-2,3,6-trimethylbenzyl)-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide

: 94-99-5
2,4-Dichlorobenzyl chloride

: 925440-72-8
(9aS)-8-acetyl-N-{4-[(2,4-dichlorobenzyl)oxy]-2,3,6-trimethylbenzyl}-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide

Guidance literature:: (9aS)-8-Acetyl-1,7-dihydroxy-N-(4-hydroxy-2,3,6-trimethylbenzyl)-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide; 2,4-Dichlorobenzyl chloride; With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 12h;

With hydrogenchloride; In water; N,N-dimethyl-formamide; at 0 ℃;

Reference yield:

: 925442-18-8
4-[({[(9aS)-8-acetyl-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-yl]carbonyl} amino)methyl]-2,3,5-trimethylphenyl acetate

: 925440-72-8
(9aS)-8-acetyl-N-{4-[(2,4-dichlorobenzyl)oxy]-2,3,6-trimethylbenzyl}-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide; water / tetrahydrofuran / 1 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 60 °C

2.2: 0 °C

With sodium hydroxide; water; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;