4-[({[(9aS)-8-acetyl-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-yl]carbonyl} amino)methyl]-2,3,5-trimethylphenyl acetate

Base Information

Chemical Name:4-[({[(9aS)-8-acetyl-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-yl]carbonyl} amino)methyl]-2,3,5-trimethylphenyl acetate
CAS No.:925442-18-8
Molecular Formula:C₂₉H₂₉NO₉
Molecular Weight:535.551
Hs Code.:

4-[({[(9aS)-8-acetyl-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-yl]carbonyl} amino)methyl]-2,3,5-trimethylphenyl acetate

Synonyms:4-[({[(9aS)-8-acetyl-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-yl]carbonyl} amino)methyl]-2,3,5-trimethylphenyl acetate

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Chemical Property of 4-[({[(9aS)-8-acetyl-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-yl]carbonyl} amino)methyl]-2,3,5-trimethylphenyl acetate

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Technology Process of 4-[({[(9aS)-8-acetyl-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-yl]carbonyl} amino)methyl]-2,3,5-trimethylphenyl acetate

There total 1 articles about 4-[({[(9aS)-8-acetyl-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-yl]carbonyl} amino)methyl]-2,3,5-trimethylphenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 925442-18-8
4-[({[(9aS)-8-acetyl-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-yl]carbonyl} amino)methyl]-2,3,5-trimethylphenyl acetate

Guidance literature:

Reference yield: 90.0%

: 925442-18-8
4-[({[(9aS)-8-acetyl-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-yl]carbonyl} amino)methyl]-2,3,5-trimethylphenyl acetate

: 925440-61-5
(9aS)-8-Acetyl-1,7-dihydroxy-N-(4-hydroxy-2,3,6-trimethylbenzyl)-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide

Guidance literature:: 4-[({[(9aS)-8-acetyl-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-yl]carbonyl} amino)methyl]-2,3,5-trimethylphenyl acetate; With sodium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; water;

Reference yield:

: 925442-18-8
4-[({[(9aS)-8-acetyl-1,7-dihydroxy-3-methoxy-9a-methyl-9-oxo-9,9a-dihydrodibenzo[b,d]furan-4-yl]carbonyl} amino)methyl]-2,3,5-trimethylphenyl acetate

: 925440-92-2
(9aS)-1,7-Dihydroxy-3-methoxy-9a-methyl-N-(4-hydroxy-2,3,6-trimethylbenzyl)-9-oxo-8-[(1E)-N-(prop-2-ynyloxy)ethaneimidoyl]-9,9a-dihydrodibenzo[b,d]furan-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / tetrahydrofuran / 1 h / 20 °C

2: sodium hydrogencarbonate / tetrahydrofuran; methanol / 4 h / 20 °C

With sodium hydroxide; water; sodium hydrogencarbonate; In tetrahydrofuran; methanol;