(2R,3S,4S,5R,6R)-5-Acetoxy-4-benzyloxy-6-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-3-hydroxy-tetrahydro-pyran-2-carboxylic acid methyl ester

Base Information

Chemical Name:(2R,3S,4S,5R,6R)-5-Acetoxy-4-benzyloxy-6-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-3-hydroxy-tetrahydro-pyran-2-carboxylic acid methyl ester
CAS No.:110255-42-0
Molecular Formula:C₄₅H₅₁NO₁₄
Molecular Weight:829.898
Hs Code.:

(2R,3S,4S,5R,6R)-5-Acetoxy-4-benzyloxy-6-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-3-hydroxy-tetrahydro-pyran-2-carboxylic acid methyl ester

Synonyms:(2R,3S,4S,5R,6R)-5-Acetoxy-4-benzyloxy-6-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-3-hydroxy-tetrahydro-pyran-2-carboxylic acid methyl ester

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Chemical Property of (2R,3S,4S,5R,6R)-5-Acetoxy-4-benzyloxy-6-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-3-hydroxy-tetrahydro-pyran-2-carboxylic acid methyl ester

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Technology Process of (2R,3S,4S,5R,6R)-5-Acetoxy-4-benzyloxy-6-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-3-hydroxy-tetrahydro-pyran-2-carboxylic acid methyl ester

There total 21 articles about (2R,3S,4S,5R,6R)-5-Acetoxy-4-benzyloxy-6-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-3-hydroxy-tetrahydro-pyran-2-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110236-57-2
Acetic acid (2S,3R,4S,5R,6S)-5-acetoxy-6-acetoxymethyl-4-benzyloxy-2-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-tetrahydro-pyran-3-yl ester

: 110255-42-0
(2R,3S,4S,5R,6R)-5-Acetoxy-4-benzyloxy-6-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-3-hydroxy-tetrahydro-pyran-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: NaOMe; MeOH

2: CSA / acetone

3: DMAP; pyridine / CH₂Cl₂

4: aq. AcOH

5: 2,2,6,6-tetramethyl-1-piperidinyloxy radical; NaClO; KBr

6: NaClO₂; aq. NaH₂PO₄

With pyridine; methanol; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite; sodium dihydrogenphosphate; camphor-10-sulfonic acid; sodium methylate; acetic acid; potassium bromide; In dichloromethane; acetone; 1: Deacetylation / 2: Acetalization / 3: Acetylation / 4: Hydrolysis / 5: Oxidation / 6: Oxidation / 7: Esterification;
DOI:10.1016/S0960-894X(99)00550-8

Reference yield:

: 110236-56-1
methyl N-benzyloxycarbonyl-2-deoxy-3,6-di-O-benzylglucopyranoside

: 110255-42-0
(2R,3S,4S,5R,6R)-5-Acetoxy-4-benzyloxy-6-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-3-hydroxy-tetrahydro-pyran-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 83 percent / Sn(OTf)2 / CH₂Cl₂ / 0 °C

2: NaOMe; MeOH

3: CSA / acetone

4: DMAP; pyridine / CH₂Cl₂

5: aq. AcOH

6: 2,2,6,6-tetramethyl-1-piperidinyloxy radical; NaClO; KBr

7: NaClO₂; aq. NaH₂PO₄

With pyridine; methanol; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite; sodium dihydrogenphosphate; tin(II) trifluoromethanesulfonate; camphor-10-sulfonic acid; sodium methylate; acetic acid; potassium bromide; In dichloromethane; acetone; 1: Glycosidation / 2: Deacetylation / 3: Acetalization / 4: Acetylation / 5: Hydrolysis / 6: Oxidation / 7: Oxidation / 8: Esterification;
DOI:10.1016/S0960-894X(99)00550-8

Reference yield:

: 110236-58-3
Methyl-3,6-di-O-benzyl-4-O-(3-O-benzyl-α-L-idopyranosyl)-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

: 110255-42-0
(2R,3S,4S,5R,6R)-5-Acetoxy-4-benzyloxy-6-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-3-hydroxy-tetrahydro-pyran-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: CSA / acetone

2: DMAP; pyridine / CH₂Cl₂

3: aq. AcOH

4: 2,2,6,6-tetramethyl-1-piperidinyloxy radical; NaClO; KBr

5: NaClO₂; aq. NaH₂PO₄

With pyridine; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite; sodium dihydrogenphosphate; camphor-10-sulfonic acid; acetic acid; potassium bromide; In dichloromethane; acetone; 1: Acetalization / 2: Acetylation / 3: Hydrolysis / 4: Oxidation / 5: Oxidation / 6: Esterification;
DOI:10.1016/S0960-894X(99)00550-8