methyl N'-4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenylcarbamimidothioate monohydroiodide

Base Information

Chemical Name:methyl N'-4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenylcarbamimidothioate monohydroiodide
CAS No.:1235491-91-4
Molecular Formula:C₁₂H₁₃ClN₄OS*HI
Molecular Weight:424.693
Hs Code.:

Synonyms:methyl N'-4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenylcarbamimidothioate monohydroiodide

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Chemical Property of methyl N'-4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenylcarbamimidothioate monohydroiodide

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Technology Process of methyl N'-4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenylcarbamimidothioate monohydroiodide

There total 1 articles about methyl N'-4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenylcarbamimidothioate monohydroiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1235491-95-8
1-(4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenyl)thiourea

: 74-88-4
methyl iodide

: 1235491-91-4
methyl N'-4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenylcarbamimidothioate monohydroiodide

Guidance literature:: In ethanol; at 70 ℃; for 3h;

Reference yield: 84.0%

: 1235492-94-0
2-(4-chlorobutyl)-1,3-dithiane-2-carboxylic acid

: 1235491-91-4
methyl N'-4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenylcarbamimidothioate monohydroiodide

: 1235495-15-4
methyl N-4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenyl-N'-(2-(4-chlorobutyl)-1,3-dithiane-2-carbonyl)carbamimidothioate

Guidance literature:: 2-(4-chlorobutyl)-1,3-dithiane-2-carboxylic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.25h;

methyl N'-4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenylcarbamimidothioate monohydroiodide; In dichloromethane; at 20 ℃; for 16h;

Reference yield: 60.0%

: 1235491-91-4
methyl N'-4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenylcarbamimidothioate monohydroiodide

: 51230-93-4
2-(4-fluorophenyl)pent-4-enoic acid

: 1235493-42-1
methyl N-4-(4-chloro-1H-imidazol-1-yl)-3-methoxyphenyl-N'-(2-(4-fluorophenyl)pent-4-enoyl)carbamimidothioate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere of nitrogen;