(1R,2S,3R)-3-[N-phenylsulfonyl-N-(3,5-dimethylphenyl)amino]-2-bornanyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanoate

Base Information

Chemical Name:(1R,2S,3R)-3-[N-phenylsulfonyl-N-(3,5-dimethylphenyl)amino]-2-bornanyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanoate
CAS No.:653595-66-5
Molecular Formula:C₃₇H₄₂F₃N₃O₁₁S₂
Molecular Weight:825.881
Hs Code.:

(1R,2S,3R)-3-[N-phenylsulfonyl-N-(3,5-dimethylphenyl)amino]-2-bornanyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanoate

Synonyms:(1R,2S,3R)-3-[N-phenylsulfonyl-N-(3,5-dimethylphenyl)amino]-2-bornanyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanoate

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Chemical Property of (1R,2S,3R)-3-[N-phenylsulfonyl-N-(3,5-dimethylphenyl)amino]-2-bornanyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanoate

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Technology Process of (1R,2S,3R)-3-[N-phenylsulfonyl-N-(3,5-dimethylphenyl)amino]-2-bornanyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanoate

There total 2 articles about (1R,2S,3R)-3-[N-phenylsulfonyl-N-(3,5-dimethylphenyl)amino]-2-bornanyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2955-74-0
ethyl N-{[(4-nitrobenzene)sulfonyl]oxy}carbamate

: 653595-54-1
(+)-(1R,2S,3R)-3-[N-phenylsulfonyl-N-(3,5-dimethylphenyl)amino]-2-bornanyl 2-(trifluoromethyl)acrylate

: 653595-66-5
(1R,2S,3R)-3-[N-phenylsulfonyl-N-(3,5-dimethylphenyl)amino]-2-bornanyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanoate

Guidance literature:: With calcium oxide; In dichloromethane; at 25 ℃; for 3h;
DOI:10.1021/ol0361554

Reference yield:

: 87420-26-6
(1R,2S,3R)-3-[N-Phenylsulfonyl-N-(3,5-dimethylphenyl)amino]bornan-2-ol

: 653595-66-5
(1R,2S,3R)-3-[N-phenylsulfonyl-N-(3,5-dimethylphenyl)amino]-2-bornanyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: 81 percent / CaO / CH₂Cl₂ / 3 h / 25 °C

With pyridine; calcium oxide; In dichloromethane; 2: aza-Michael addition;
DOI:10.1021/ol0361554