(E)-1-(4-fluorophenyl)ethanone O-benzyl oxime

Base Information

Chemical Name:(E)-1-(4-fluorophenyl)ethanone O-benzyl oxime
CAS No.:1384454-53-8
Molecular Formula:C₁₅H₁₄FNO
Molecular Weight:243.281
Hs Code.:

Synonyms:(E)-1-(4-fluorophenyl)ethanone O-benzyl oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(4-fluorophenyl)ethanone O-benzyl oxime

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of (E)-1-(4-fluorophenyl)ethanone O-benzyl oxime

There total 3 articles about (E)-1-(4-fluorophenyl)ethanone O-benzyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 100-44-7
benzyl chloride

: 158364-41-1
(E)-1-(4-fluorophenyl)ethan-1-one oxime

: 1384454-53-8
(E)-1-(4-fluorophenyl)ethanone O-benzyl oxime

Guidance literature:: (E)-1-(4-fluorophenyl)ethan-1-one oxime; With sodium hydride; In N,N-dimethyl-formamide; for 24h; Cooling with ice;

benzyl chloride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.tetasy.2012.05.008

Reference yield: 80.0%

: 100-39-0
benzyl bromide

: 158364-41-1
(E)-1-(4-fluorophenyl)ethan-1-one oxime

: 1384454-53-8
(E)-1-(4-fluorophenyl)ethanone O-benzyl oxime

Guidance literature:: (E)-1-(4-fluorophenyl)ethan-1-one oxime; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

benzyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.1021/jo400371x

Reference yield:

: 403-42-9
1-(4-fluorophenyl)ethanone

: 1384454-53-8
(E)-1-(4-fluorophenyl)ethanone O-benzyl oxime

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine hydrochloride; sodium acetate / ethanol / 5 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 24 h / Cooling with ice

2.2: 20 °C

With hydroxylamine hydrochloride; sodium acetate; sodium hydride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2012.05.008