C₂₆H₂₅N₃O₅

Base Information

Chemical Name:C₂₆H₂₅N₃O₅
CAS No.:1177423-36-7
Molecular Formula:C₂₆H₂₅N₃O₅
Molecular Weight:459.502
Hs Code.:

C<sub>26</sub>H<sub>25</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₂₆H₂₅N₃O₅

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Chemical Property of C₂₆H₂₅N₃O₅

Chemical Property:

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Technology Process of C₂₆H₂₅N₃O₅

There total 11 articles about C₂₆H₂₅N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1177423-34-5
C₂₇H₂₇N₃O₅

: 1177423-36-7
C₂₆H₂₅N₃O₅

Guidance literature:: C₂₇H₂₇N₃O₅; With sodium hydroxide; In tetrahydrofuran; methanol; for 1h; Reflux; Heating;

With hydrogenchloride; In water; pH=~ 2;

Reference yield:

: 1177423-29-8
C₂₄H₂₂N₂O₅

: 1177423-36-7
C₂₆H₂₅N₃O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; sodium hydroxide / tetrahydrofuran; methanol; dichloromethane / 4 h / 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 0.08 h / 20 °C

2.2: 13 h

3.1: sodium hydroxide / tetrahydrofuran; methanol / 1 h / Reflux; Heating

3.2: pH ~ 2

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 98273-79-1
3-chloropyridine-4-carboxylic acid methyl ester

: 1177423-36-7
C₂₆H₂₅N₃O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 1 h / -78 °C

2.1: acetic acid / N,N-dimethyl-formamide / 62 h / 140 °C

3.1: sodium tetrahydroborate / methanol; dichloromethane / 3 h / 0 °C

4.1: dmap / dichloromethane / 0 - 20 °C

5.1: titanium tetrachloride / dichloromethane / 0.08 h / 0 °C

5.2: 1 h / 0 °C

6.1: water; sodium hydroxide / tetrahydrofuran; methanol; dichloromethane / 4 h / 20 °C

7.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 0.08 h / 20 °C

7.2: 13 h

8.1: sodium hydroxide / tetrahydrofuran; methanol / 1 h / Reflux; Heating

8.2: pH ~ 2

With dmap; sodium tetrahydroborate; n-butyllithium; water; titanium tetrachloride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diisopropylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide;