tetraphenylphosphonium oxopentacyanomolybdate(IV)

Base Information

Chemical Name:tetraphenylphosphonium oxopentacyanomolybdate(IV)
CAS No.:86568-26-5
Molecular Formula:C₅MoN₅O*3C₂₄H₂₀P
Molecular Weight:1260.22
Hs Code.:

Synonyms:tetraphenylphosphonium oxopentacyanomolybdate(IV)

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Chemical Property of tetraphenylphosphonium oxopentacyanomolybdate(IV)

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Technology Process of tetraphenylphosphonium oxopentacyanomolybdate(IV)

There total 2 articles about tetraphenylphosphonium oxopentacyanomolybdate(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 115436-94-7
potassium oxopentacyanomolybdate(IV) dihydrate

: 2001-45-8
tetraphenyl phosphonium chloride

: 86568-26-5
tetraphenylphosphonium oxopentacyanomolybdate(IV)

Guidance literature:: In dichloromethane; water; addn. of PPh4Cl to Mo-complex in two-phase system CH2Cl2/H2O, stirring (5 min), decantation of org. solvent, drying (over MgSO4); recrystn. (acetonitrile/diethyl ether, -30°C); elem. anal.;

Reference yield:

: 115509-89-2
tetraphenylphosphonium oxoperoxotetracyanomolybdate(VI)

: 603-35-0
triphenylphosphine

: 67168-41-6
(PPh₄)4Mo₈O₂₆

: 115436-95-8
2P(C₆H₅)4⁽¹⁺⁾*Mo₂O₇^(2-)={P(C₆H₅)4}2{Mo₂O₇}

: 86568-26-5
tetraphenylphosphonium oxopentacyanomolybdate(IV)

: 791-28-6
Triphenylphosphine oxide

Guidance literature:: In acetonitrile; Ar-atmosphere, 25°C, ratio Mo-complex/PPh3 0.5 ((31)P-NMR-monitoring of OPPh3); sepn. of solid (filtration), evapn. of filtrate; IR spectroscopy;

Reference yield: 98.0%

: 86568-26-5
tetraphenylphosphonium oxopentacyanomolybdate(IV)

: 611-23-4
2-nitrosotoluene

: tetraphenylphosphonium tetracyanooxo{N-o-tplylhydroxyaminato^(2-)-O,N}molybdate(VI)

Guidance literature:: In dichloromethane; react. at 243 K, warming up to 298 K within 1 h, pptn. on addn. of ether; recrystn. (acetonitrile/diethyl ether (60/40)), elem. anal.;