C₃₁H₄₆N₄O

Base Information

Chemical Name:C₃₁H₄₆N₄O
CAS No.:863561-73-3
Molecular Formula:C₃₁H₄₆N₄O
Molecular Weight:490.732
Hs Code.:

C<sub>31</sub>H<sub>46</sub>N<sub>4</sub>O

Synonyms:C₃₁H₄₆N₄O

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Chemical Property of C₃₁H₄₆N₄O

Chemical Property:

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Technology Process of C₃₁H₄₆N₄O

There total 14 articles about C₃₁H₄₆N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 863561-74-4
C₃₈H₄₈N₄OS

: 863561-73-3
C₃₁H₄₆N₄O

Guidance literature:: With hydrogen; nickel; In methanol; ethanol; at 20 ℃; for 2h; under 1292.09 Torr;

Reference yield:

: 666852-63-7
ethyl 2-methyl-2-(2-thienyl)propanoate

: 863561-73-3
C₃₁H₄₆N₄O

Guidance literature:: Multi-step reaction with 10 steps

1.1: nitronium tetrafluoborate / 1,2-dimethoxyethane / 4 h / -55 - -10 °C

2.1: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 5 h / 1140.08 Torr

3.1: tetrahydrofuran / 16 h / Heating / reflux

4.1: sodium hydroxide; water / ethanol / 1.5 h / Heating / reflux

5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h

5.2: 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h

6.2: 5 - 20 °C

7.1: hydrogenchloride / 1,4-dioxane; iso-butanol / 1 h / 90 °C

8.1: hydrazine / ethanol / 16 h / 20 °C

9.1: sodium cyanoborohydride / acetic acid / methanol

10.1: hydrogen / nickel / methanol; ethanol / 2 h / 20 °C / 1292.09 Torr

With hydrogenchloride; dmap; sodium hydroxide; nitronium tetrafluoborate; water; hydrogen; sodium hydride; sodium cyanoborohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydrazine; palladium 10% on activated carbon; nickel; acetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; iso-butanol;

Reference yield:

: 1000819-06-6
C₁₀H₁₅NO₂S

: 863561-73-3
C₃₁H₄₆N₄O

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrahydrofuran / 16 h / Heating / reflux

2.1: sodium hydroxide; water / ethanol / 1.5 h / Heating / reflux

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h

3.2: 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h

4.2: 5 - 20 °C

5.1: hydrogenchloride / 1,4-dioxane; iso-butanol / 1 h / 90 °C

6.1: hydrazine / ethanol / 16 h / 20 °C

7.1: sodium cyanoborohydride / acetic acid / methanol

8.1: hydrogen / nickel / methanol; ethanol / 2 h / 20 °C / 1292.09 Torr

With hydrogenchloride; dmap; sodium hydroxide; water; hydrogen; sodium hydride; sodium cyanoborohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydrazine; nickel; acetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; iso-butanol;