all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-[6-N-(benzyloxycarbonyl)aminohexyl]-1,3,5-triaminocyclohexane

Base Information

Chemical Name:all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-[6-N-(benzyloxycarbonyl)aminohexyl]-1,3,5-triaminocyclohexane
CAS No.:688790-66-1
Molecular Formula:C₃₀H₅₀N₄O₆
Molecular Weight:562.75
Hs Code.:

Synonyms:all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-[6-N-(benzyloxycarbonyl)aminohexyl]-1,3,5-triaminocyclohexane

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Chemical Property of all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-[6-N-(benzyloxycarbonyl)aminohexyl]-1,3,5-triaminocyclohexane

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Technology Process of all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-[6-N-(benzyloxycarbonyl)aminohexyl]-1,3,5-triaminocyclohexane

There total 5 articles about all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-[6-N-(benzyloxycarbonyl)aminohexyl]-1,3,5-triaminocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 116784-97-5
N-benzyloxycarbonyl-6-bromo-1-hexylamine

: 688790-64-9
all-cis-1,3-N,N'-(di-tert-butyloxycarbonyl)-1,3,5-triaminocyclohexane

: 688790-66-1
all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-[6-N-(benzyloxycarbonyl)aminohexyl]-1,3,5-triaminocyclohexane

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; for 192h; pH=8; Heating;
DOI:10.1021/ja039465q

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 688790-66-1
all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-[6-N-(benzyloxycarbonyl)aminohexyl]-1,3,5-triaminocyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / triethylamine / methanol / 10 h / 20 °C

2: 84 percent / CBr₄; PPh₃ / CH₂Cl₂ / 0 - 20 °C

3: 38 percent / diisopropylethylamine / acetonitrile / 192 h / pH 8 / Heating

With carbon tetrabromide; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja039465q

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 688790-66-1
all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-[6-N-(benzyloxycarbonyl)aminohexyl]-1,3,5-triaminocyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / triethylamine / methanol / 48 h / 20 °C

2: 38 percent / diisopropylethylamine / acetonitrile / 192 h / pH 8 / Heating

With triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; acetonitrile;
DOI:10.1021/ja039465q