(1R,2R,3S)-1,2-O-dibenzyl-4-triphenylmethyl-1-<1'-triphenylmethyl-1'H-imidazol-4'-yl>butane-1,2,3,4-tetrol

Base Information

Chemical Name:(1R,2R,3S)-1,2-O-dibenzyl-4-triphenylmethyl-1-<1'-triphenylmethyl-1'H-imidazol-4'-yl>butane-1,2,3,4-tetrol
CAS No.:607357-20-0
Molecular Formula:C₅₉H₅₂N₂O₄
Molecular Weight:853.073
Hs Code.:

Synonyms:(1R,2R,3S)-1,2-O-dibenzyl-4-triphenylmethyl-1-<1'-triphenylmethyl-1'H-imidazol-4'-yl>butane-1,2,3,4-tetrol

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Chemical Property of (1R,2R,3S)-1,2-O-dibenzyl-4-triphenylmethyl-1-<1'-triphenylmethyl-1'H-imidazol-4'-yl>butane-1,2,3,4-tetrol

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Technology Process of (1R,2R,3S)-1,2-O-dibenzyl-4-triphenylmethyl-1-<1'-triphenylmethyl-1'H-imidazol-4'-yl>butane-1,2,3,4-tetrol

There total 3 articles about (1R,2R,3S)-1,2-O-dibenzyl-4-triphenylmethyl-1-<1'-triphenylmethyl-1'H-imidazol-4'-yl>butane-1,2,3,4-tetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76-83-5
trityl chloride

: 607357-20-0
(1R,2R,3S)-1,2-O-dibenzyl-4-triphenylmethyl-1-<1'-triphenylmethyl-1'H-imidazol-4'-yl>butane-1,2,3,4-tetrol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / DMAP, pyridine / 4 h / 70 - 75 °C

2: 1.) NaH(50 percent-oil), 2.) Bu₄NI / 1.) THF, -5 deg C, 2.) THF, 0 deg C, 24 h

With pyridine; dmap; tetra-(n-butyl)ammonium iodide; sodium hydride;
DOI:10.1002/(SICI)1099-0690(199904)1999:4<893::AID-EJOC893>3.0.CO;2-#

Reference yield:

: 172016-35-2
4⁽⁵⁾-(L-xylotetritol-1-yl)imidazole

: 607357-20-0
(1R,2R,3S)-1,2-O-dibenzyl-4-triphenylmethyl-1-<1'-triphenylmethyl-1'H-imidazol-4'-yl>butane-1,2,3,4-tetrol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / DMAP, pyridine / 4 h / 70 - 75 °C

2: 1.) NaH(50 percent-oil), 2.) Bu₄NI / 1.) THF, -5 deg C, 2.) THF, 0 deg C, 24 h

With pyridine; dmap; tetra-(n-butyl)ammonium iodide; sodium hydride;
DOI:10.1002/(SICI)1099-0690(199904)1999:4<893::AID-EJOC893>3.0.CO;2-#

Reference yield:

: 100-39-0
benzyl bromide

: (1R,2S,3S)-4-O-triphenylmethyl-1-<1'-(triphenylmethyl)-1'H-imidazol-4'-yl>butane-1,2,3,4-tetrol

: 607357-20-0
(1R,2R,3S)-1,2-O-dibenzyl-4-triphenylmethyl-1-<1'-triphenylmethyl-1'H-imidazol-4'-yl>butane-1,2,3,4-tetrol

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; Yield given; Multistep reaction; 1.) THF, -5 deg C, 2.) THF, 0 deg C, 24 h;
DOI:10.1002/(SICI)1099-0690(199904)1999:4<893::AID-EJOC893>3.0.CO;2-#