C₁₇H₂₆O₄

Base Information

• Chemical Name: C₁₇H₂₆O₄
• CAS No.: 955044-10-7
• Molecular Formula: C₁₇H₂₆O₄
• Molecular Weight: 294.391
• Mol file: 955044-10-7.mol

Synonyms:C₁₇H₂₆O₄

Chemical Property of C₁₇H₂₆O₄

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₇H₂₆O₄

There total 1 articles about C₁₇H₂₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

C6H12O2 + (2S)-3-(benzyloxy)-2-methylpropanal (79027-28-4) + trifluoroacetic acid (76-05-1) → C17H26O4 (955044-10-7)

Guidance literature:

C₆H₁₂O₂; (2S)-3-(benzyloxy)-2-methylpropanal; trifluoroacetic acid; In dichloromethane;

With potassium carbonate; In methanol; at 20 ℃; for 5h; Further stages.;

DOI:10.1055/s-2007-984896

Reference yield: 86.0%

C17H26O4 (955044-10-7) + tert-butyldimethylsilyl chloride (18162-48-6) → C23H40O4Si (955044-19-6)

Guidance literature:

With 1H-imidazole; In dichloromethane; at 0 - 20 ℃; for 6h;

DOI:10.1055/s-2007-984896

Reference yield:

C17H26O4 (955044-10-7) → C24H42O4Si (955044-12-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / imidazole / CH₂Cl₂ / 6 h / 0 - 20 °C

2: 90 percent / NaH / tetrahydrofuran / 6 h / 0 - 20 °C

With 1H-imidazole; sodium hydride; In tetrahydrofuran; dichloromethane;

DOI:10.1055/s-2007-984896

upstream raw materials:

(2S)-3-(benzyloxy)-2-methylpropanal

trifluoroacetic acid

Downstream raw materials:

C₂₃H₄₀O₄Si

C₂₄H₄₂O₄Si