Technology Process of C68H74N6O13
There total 10 articles about C68H74N6O13 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C25H32O6;
With
dmap; ethylene dichloride hydrochloride;
In
dichloromethane;
for 0.25h;
(2S,3R)-benzyl 3-hydroxy-2-(3-(9-((3R,4S,5R)-3,4,5-tris(benzyloxy)tetrahydro-2H-pyran-2-yl)-9H-purin-6-yl)ureido)butanoate;
In
dichloromethane;
for 12h;
DOI:10.1002/anie.201206797
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: Dess-Martin periodane / dichloromethane / 5 h
2.1: sodium tetrahydroborate / methanol; dichloromethane / 0.17 h
3.1: lithium hydroxide / tetrahydrofuran; water; 1,4-dioxane / 3 h / 60 °C
4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 0 °C
5.1: sodium periodate; ruthenium(III) trichloride hydrate / water; dichloromethane; acetonitrile / 1.75 h
6.1: ethylene dichloride hydrochloride; dmap / dichloromethane / 0.25 h
6.2: 12 h
With
dmap; sodium tetrahydroborate; sodium periodate; ethylene dichloride hydrochloride; ruthenium(III) trichloride hydrate; sodium hydride; Dess-Martin periodane; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1002/anie.201206797
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hydroxide / tetrahydrofuran; water; 1,4-dioxane / 3 h / 60 °C
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 0 °C
3.1: sodium periodate; ruthenium(III) trichloride hydrate / water; dichloromethane; acetonitrile / 1.75 h
4.1: ethylene dichloride hydrochloride; dmap / dichloromethane / 0.25 h
4.2: 12 h
With
dmap; sodium periodate; ethylene dichloride hydrochloride; ruthenium(III) trichloride hydrate; sodium hydride; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1002/anie.201206797
