N-(3-bromopropyl)-N-(diethoxyphosphoryl)-O-benzylhydroxylamine

Base Information

• Chemical Name: N-(3-bromopropyl)-N-(diethoxyphosphoryl)-O-benzylhydroxylamine
• CAS No.: 650635-21-5
• Molecular Formula: C₁₄H₂₃BrNO₄P
• Molecular Weight: 380.219
• Mol file: 650635-21-5.mol

Synonyms:N-(3-bromopropyl)-N-(diethoxyphosphoryl)-O-benzylhydroxylamine

Chemical Property of N-(3-bromopropyl)-N-(diethoxyphosphoryl)-O-benzylhydroxylamine

Chemical Property:

Purity/Quality:

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Technology Process of N-(3-bromopropyl)-N-(diethoxyphosphoryl)-O-benzylhydroxylamine

There total 1 articles about N-(3-bromopropyl)-N-(diethoxyphosphoryl)-O-benzylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

N-(diethoxyphosphoryl)-O-benzylhydroxylamine (57943-11-0) + 1,3-dibromo-propane (109-64-8) → N-(3-bromopropyl)-N-(diethoxyphosphoryl)-O-benzylhydroxylamine (650635-21-5)

Guidance literature:

With tetrabutylammomium bromide; sodium hydride; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1016/j.tet.2003.10.056

Reference yield: 92.0%

N-(3-bromopropyl)-N-(diethoxyphosphoryl)-O-benzylhydroxylamine (650635-21-5) → N-(3-bromopropyl)-O-benzylhydroxylamine hydrochloride

Guidance literature:

With hydrogenchloride; In ethanol; for 0.0833333h; Heating;

DOI:10.1016/j.tet.2003.10.056

Reference yield: 73.0%

N-(diethoxyphosphoryl)-O-benzylhydroxylamine (57943-11-0) + N-(3-bromopropyl)-N-(diethoxyphosphoryl)-O-benzylhydroxylamine (650635-21-5) → 1,3-bis-(O-benzyloxy-N-diethoxyphosphorylamino)propane

Guidance literature:

With tetrabutylammomium bromide; sodium hydride; In tetrahydrofuran; at 20 ℃; for 5h;

DOI:10.1016/j.tet.2003.10.056

upstream raw materials:

N-(diethoxyphosphoryl)-O-benzylhydroxylamine

1,3-dibromo-propane