C₃₃H₅₈O₂Si₂

Base Information

Chemical Name:C₃₃H₅₈O₂Si₂
CAS No.:1395881-52-3
Molecular Formula:C₃₃H₅₈O₂Si₂
Molecular Weight:542.993
Hs Code.:

C<sub>33</sub>H<sub>58</sub>O<sub>2</sub>Si<sub>2</sub>

Synonyms:C₃₃H₅₈O₂Si₂

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Chemical Property of C₃₃H₅₈O₂Si₂

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Technology Process of C₃₃H₅₈O₂Si₂

There total 9 articles about C₃₃H₅₈O₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1395881-51-2
C₃₃H₅₈O₃Si₂

: 1395881-52-3
C₃₃H₅₈O₂Si₂

Guidance literature:: With ammonia; lithium; In tetrahydrofuran; at -78 ℃; for 0.25h;
DOI:10.1021/ol301715u DOI:10.1021/ol301715u

Reference yield:

: (1R,2S)-1-(2-acetoxyethyl)-1,2,5,5-tetramethyl-Δ^4a(8a)-octahydronaphthalene

: 1395881-52-3
C₃₃H₅₈O₂Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydroxide / methanol / 0.5 h / 20 °C

2.1: tributylphosphine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.1: dihydrogen peroxide; water / tetrahydrofuran / 0.75 h / 50 °C

4.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / acetone; water / 36 h / 20 °C

5.1: sodium periodate / tetrahydrofuran; water / 0.5 h / 20 °C

6.1: tert.-butyl lithium / diethyl ether / 0.5 h / -78 °C / Inert atmosphere

6.2: -78 - 20 °C / Inert atmosphere

7.1: lithium; ammonia / tetrahydrofuran / 0.25 h / -78 °C

With sodium periodate; osmium(VIII) oxide; tributylphosphine; ammonia; water; dihydrogen peroxide; tert.-butyl lithium; lithium; 4-methylmorpholine N-oxide; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; water; acetone;
DOI:10.1021/ol301715u DOI:10.1021/ol301715u

Reference yield:

: 64061-39-8
(1R,2R,4aS,8aS)-(+)-1-(2'-acetoxyethyl)-1,2,3,4,4a,5,6,7,8,8a-decahydro-2-hydroxy-2,5,5,8a-tetramethylnaphthalene

: 1395881-52-3
C₃₃H₅₈O₂Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 12 h / 20 °C

2.1: potassium hydroxide / methanol / 0.5 h / 20 °C

3.1: tributylphosphine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

4.1: dihydrogen peroxide; water / tetrahydrofuran / 0.75 h / 50 °C

5.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / acetone; water / 36 h / 20 °C

6.1: sodium periodate / tetrahydrofuran; water / 0.5 h / 20 °C

7.1: tert.-butyl lithium / diethyl ether / 0.5 h / -78 °C / Inert atmosphere

7.2: -78 - 20 °C / Inert atmosphere

8.1: lithium; ammonia / tetrahydrofuran / 0.25 h / -78 °C

With sodium periodate; osmium(VIII) oxide; tributylphosphine; boron trifluoride diethyl etherate; ammonia; water; dihydrogen peroxide; tert.-butyl lithium; lithium; 4-methylmorpholine N-oxide; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone;
DOI:10.1021/ol301715u DOI:10.1021/ol301715u