thexyldimethylsilyl O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:thexyldimethylsilyl O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:228563-39-1
Molecular Formula:C₄₈H₆₃N₃O₉Si
Molecular Weight:854.128
Hs Code.:

Synonyms:thexyldimethylsilyl O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of thexyldimethylsilyl O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of thexyldimethylsilyl O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 4 articles about thexyldimethylsilyl O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 157488-87-4
thexyldimethylsilyl O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 228563-39-1
thexyldimethylsilyl O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With hydrogenchloride; molecular sieve; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether;

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 228563-39-1
thexyldimethylsilyl O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / p-TsOH / acetonitrile / 1 h / 20 °C

2: 85 percent / TMSOTf / diethyl ether

3: 80 percent / NaCNBH₃; HCl; molecular sieves / tetrahydrofuran; diethyl ether

With hydrogenchloride; molecular sieve; sodium cyanoborohydride; toluene-4-sulfonic acid; trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; diethyl ether; acetonitrile; 1: Substitution / 2: Substitution / 3: Reduction;

Reference yield:

: 157488-91-0
thexyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 228563-39-1
thexyldimethylsilyl O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / TMSOTf / diethyl ether

2: 80 percent / NaCNBH₃; HCl; molecular sieves / tetrahydrofuran; diethyl ether

With hydrogenchloride; molecular sieve; sodium cyanoborohydride; trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; diethyl ether; 1: Substitution / 2: Reduction;