N-[2-(aminomethyl)-3,3,3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide

Base Information

Chemical Name:N-[2-(aminomethyl)-3,3,3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide
CAS No.:960249-98-3
Molecular Formula:C₁₁H₁₁Cl₂F₃N₂O₂
Molecular Weight:331.122
Hs Code.:

Synonyms:N-[2-(aminomethyl)-3,3,3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide

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Chemical Property of N-[2-(aminomethyl)-3,3,3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide

Chemical Property:

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Technology Process of N-[2-(aminomethyl)-3,3,3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide

There total 2 articles about N-[2-(aminomethyl)-3,3,3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 960249-97-2
N-[2-(azidomethyl)-3,3.3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide

: 960249-98-3
N-[2-(aminomethyl)-3,3,3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide

Guidance literature:: N-[2-(azidomethyl)-3,3.3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide; With polymer bound triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 19h;

With water; In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield:

: 960249-96-1
1,1-dimethylethyl [(2,6-dichlorophenyl)carbonyl]{[2-(trifluoromethyl)-2-oxiranyl]methyl}carbamate

: 960249-98-3
N-[2-(aminomethyl)-3,3,3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium azide / water; N,N-dimethyl-formamide / 20 °C

2.1: polymer bound triphenylphosphine / tetrahydrofuran / 19 h / 20 °C

2.2: 24 h / 20 °C

With sodium azide; polymer bound triphenylphosphine; In tetrahydrofuran; water; N,N-dimethyl-formamide;