N-[2-(azidomethyl)-3,3.3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide

Base Information

• Chemical Name: N-[2-(azidomethyl)-3,3.3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide
• CAS No.: 960249-97-2
• Molecular Formula: C₁₁H₉Cl₂F₃N₄O₂
• Molecular Weight: 357.119
• Mol file: 960249-97-2.mol

Synonyms:N-[2-(azidomethyl)-3,3.3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide

Chemical Property of N-[2-(azidomethyl)-3,3.3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[2-(azidomethyl)-3,3.3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide

There total 1 articles about N-[2-(azidomethyl)-3,3.3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-dimethylethyl [(2,6-dichlorophenyl)carbonyl]{[2-(trifluoromethyl)-2-oxiranyl]methyl}carbamate (960249-96-1) → N-[2-(azidomethyl)-3,3.3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide (960249-97-2)

Guidance literature:

With sodium azide; In water; N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

N-[2-(azidomethyl)-3,3.3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide (960249-97-2) → N-[2-(aminomethyl)-3,3,3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide (960249-98-3)

Guidance literature:

N-[2-(azidomethyl)-3,3.3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide; With polymer bound triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 19h;

With water; In tetrahydrofuran; at 20 ℃; for 24h;

upstream raw materials:

1,1-dimethylethyl [(2,6-dichlorophenyl)carbonyl]{[2-(trifluoromethyl)-2-oxiranyl]methyl}carbamate

Downstream raw materials:

N-[2-(aminomethyl)-3,3,3-trifluoro-2-hydroxypropyl]-2,6-dichlorobenzamide