1-(1-benzyl-piperidin-4-yl)-3-4-(methylsulfinyl)butyl thiourea

Base Information

Chemical Name:1-(1-benzyl-piperidin-4-yl)-3-4-(methylsulfinyl)butyl thiourea
CAS No.:1356346-85-4
Molecular Formula:C₁₈H₂₉N₃OS₂
Molecular Weight:367.58
Hs Code.:

Synonyms:1-(1-benzyl-piperidin-4-yl)-3-4-(methylsulfinyl)butyl thiourea

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Chemical Property of 1-(1-benzyl-piperidin-4-yl)-3-4-(methylsulfinyl)butyl thiourea

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Technology Process of 1-(1-benzyl-piperidin-4-yl)-3-4-(methylsulfinyl)butyl thiourea

There total 4 articles about 1-(1-benzyl-piperidin-4-yl)-3-4-(methylsulfinyl)butyl thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 50541-93-0
4-amino-1-benzylpiperidine

: 4478-93-7
D,L-sulforaphane

: 1356346-85-4
1-(1-benzyl-piperidin-4-yl)-3-4-(methylsulfinyl)butyl thiourea

Guidance literature:: In dichloromethane; for 1h; Reflux;

Reference yield:

: 59121-24-3
4-(methylthio)butyronitrile

: 1356346-85-4
1-(1-benzyl-piperidin-4-yl)-3-4-(methylsulfinyl)butyl thiourea

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 3 h / Inert atmosphere; Reflux

2.1: dihydrogen peroxide / 2,2,2-trifluoroethanol / 1.33 h / 0 - 20 °C / Inert atmosphere

3.1: triethylamine / ethanol / 0.5 h / 20 °C / Inert atmosphere

3.2: 2.25 h / 0 - 20 °C

4.1: dichloromethane / 1 h / Reflux

With lithium aluminium tetrahydride; dihydrogen peroxide; triethylamine; In diethyl ether; ethanol; dichloromethane; 2,2,2-trifluoroethanol;

Reference yield:

: 55021-77-7
4-(methylthio)-1-butylamine

: 1356346-85-4
1-(1-benzyl-piperidin-4-yl)-3-4-(methylsulfinyl)butyl thiourea

Guidance literature:: Multi-step reaction with 3 steps

1.1: dihydrogen peroxide / 2,2,2-trifluoroethanol / 1.33 h / 0 - 20 °C / Inert atmosphere

2.1: triethylamine / ethanol / 0.5 h / 20 °C / Inert atmosphere

2.2: 2.25 h / 0 - 20 °C

3.1: dichloromethane / 1 h / Reflux

With dihydrogen peroxide; triethylamine; In ethanol; dichloromethane; 2,2,2-trifluoroethanol;