Technology Process of C34H31NO4
There total 10 articles about C34H31NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
methanol;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium carbonate; triphenylphosphine / tetrakis(triphenylphosphine) palladium(0) / methanol; toluene / 14 h / 80 °C
2.1: hydrazine hydrate / palladium 10% on activated carbon / ethanol / 1.33 h / Reflux
3.1: triethylamine / dichloromethane / 20 °C
4.1: sodium hydride / N,N-dimethyl-formamide
5.1: tris-(o-tolyl)phosphine; silver carbonate / palladium diacetate / N,N-dimethyl-formamide / 160 °C / Inert atmosphere
6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere
6.3: 20 °C
7.1: sodium tetrahydroborate / methanol / 20 °C
With
sodium tetrahydroborate; lithium aluminium tetrahydride; sodium hydride; sodium carbonate; hydrazine hydrate; triethylamine; triphenylphosphine; tris-(o-tolyl)phosphine; silver carbonate;
tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; palladium diacetate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
5.1: Heck Reaction;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine / dichloromethane / 20 °C
2.1: sodium hydride / N,N-dimethyl-formamide
3.1: tris-(o-tolyl)phosphine; silver carbonate / palladium diacetate / N,N-dimethyl-formamide / 160 °C / Inert atmosphere
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere
4.3: 20 °C
5.1: sodium tetrahydroborate / methanol / 20 °C
With
sodium tetrahydroborate; lithium aluminium tetrahydride; sodium hydride; triethylamine; tris-(o-tolyl)phosphine; silver carbonate;
palladium diacetate;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
3.1: Heck Reaction;