4-morpholinyl p-nitrophenyl sulfoxide

Base Information

• Chemical Name: 4-morpholinyl p-nitrophenyl sulfoxide
• CAS No.: 19955-46-5
• Molecular Formula: C₁₀H₁₂N₂O₄S
• Molecular Weight: 256.282
• Mol file: 19955-46-5.mol

Synonyms:4-morpholinyl p-nitrophenyl sulfoxide

Chemical Property of 4-morpholinyl p-nitrophenyl sulfoxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 4-morpholinyl p-nitrophenyl sulfoxide

There total 3 articles about 4-morpholinyl p-nitrophenyl sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(p-nitrophenylthio)morpholine (40208-36-4) → 4-morpholinyl p-nitrophenyl sulfoxide (19955-46-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 2h; Ambient temperature;

Reference yield:

morpholine (110-91-8,99108-56-2) + 4-nitro-benzenesulfinyl chloride (13088-17-0) → 4-morpholinyl p-nitrophenyl sulfoxide (19955-46-5)

Guidance literature:

In dichloromethane; at -40 - -20 ℃;

DOI:10.1021/jo01260a031

Reference yield:

N-(p-nitrophenylthio)morpholine (40208-36-4) → 4-(4-nitrobenzenesulfonyl)morpholine (1024-30-2) + 4-morpholinyl p-nitrophenyl sulfoxide (19955-46-5)

Guidance literature:

With oxygen; In benzene; Rate constant; Irradiation; k_r (rate const. for products formation), k_T (rate const. for disappearence of singlet O₂) and k_Q (rate const. for triplet O₂ formation) were determined; sulfoxide and sulfone ratio was determined;

DOI:10.1016/0040-4039(96)01300-7

upstream raw materials:

morpholine

4-nitro-benzenesulfinyl chloride

N-(p-nitrophenylthio)morpholine