methyl 5-deoxy-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranoside

Base Information

Chemical Name:methyl 5-deoxy-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranoside
CAS No.:1583293-77-9
Molecular Formula:C₂₂H₂₄N₂O₅
Molecular Weight:396.443
Hs Code.:

Synonyms:methyl 5-deoxy-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranoside

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Chemical Property of methyl 5-deoxy-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranoside

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Technology Process of methyl 5-deoxy-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranoside

There total 3 articles about methyl 5-deoxy-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1583293-65-5
methyl 5-deoxy-2,3-O-isopropylidene-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranoside

: 1583293-77-9
methyl 5-deoxy-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranoside

: 1583293-83-7
5-deoxy-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranose

Guidance literature:: With acetic acid; In water; at 80 ℃; for 3h;
DOI:10.1007/s00706-014-1193-x

Reference yield:

: 4137-56-8
methyl 2,3-O-isopropylidene-5-O-p-tolylsulfonyl-β-D-ribofuranoside

: 1583293-77-9
methyl 5-deoxy-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranoside

: 1583293-83-7
5-deoxy-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 100 °C

1.2: 5 h / 100 °C

2.1: acetic acid / water / 3 h / 80 °C

With sodium hydride; acetic acid; In water; N,N-dimethyl-formamide;
DOI:10.1007/s00706-014-1193-x

Reference yield:

: 78751-23-2
6,7-Dimethyl-3-phenyl-1,2-dihydro-chinoxalin-2-on

: 1583293-77-9
methyl 5-deoxy-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranoside

: 1583293-83-7
5-deoxy-5-(6,7-dimethyl-2-oxo-3-phenyl-1(2H)-quinoxalinyl)-β-D-ribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 100 °C

1.2: 5 h / 100 °C

2.1: acetic acid / water / 3 h / 80 °C

With sodium hydride; acetic acid; In water; N,N-dimethyl-formamide;
DOI:10.1007/s00706-014-1193-x