4-[4-(4,6-dimethylpyrimidin-5-yl)-3-methylphenoxy]-3-methylfuro[3,2-c]pyridine

Base Information

Chemical Name:4-[4-(4,6-dimethylpyrimidin-5-yl)-3-methylphenoxy]-3-methylfuro[3,2-c]pyridine
CAS No.:1609577-45-8
Molecular Formula:C₂₁H₁₉N₃O₂
Molecular Weight:345.401
Hs Code.:

Synonyms:4-[4-(4,6-dimethylpyrimidin-5-yl)-3-methylphenoxy]-3-methylfuro[3,2-c]pyridine

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Chemical Property of 4-[4-(4,6-dimethylpyrimidin-5-yl)-3-methylphenoxy]-3-methylfuro[3,2-c]pyridine

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Technology Process of 4-[4-(4,6-dimethylpyrimidin-5-yl)-3-methylphenoxy]-3-methylfuro[3,2-c]pyridine

There total 3 articles about 4-[4-(4,6-dimethylpyrimidin-5-yl)-3-methylphenoxy]-3-methylfuro[3,2-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 13061-96-6
dihydroxy-methyl-borane

: 1609581-30-7
3-bromo-4-[4-(4,6-dimethylpyrimidin-5-yl)-3-methylphenoxy]furo[3,2-c]pyridine

: 1609577-45-8
4-[4-(4,6-dimethylpyrimidin-5-yl)-3-methylphenoxy]-3-methylfuro[3,2-c]pyridine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; ethanol; water; at 120 ℃; for 14h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 1609259-54-2
5-(4-methoxy-2-methylphenyl)-4,6-dimethylpyrimidine

: 1609577-45-8
4-[4-(4,6-dimethylpyrimidin-5-yl)-3-methylphenoxy]-3-methylfuro[3,2-c]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: boron tribromide / dichloromethane / 16 h / 20 - 70 °C

2: caesium carbonate / dimethyl sulfoxide / 3 h / 120 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane; water; ethanol / 14 h / 120 °C / Inert atmosphere; Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; sodium carbonate; caesium carbonate; In 1,4-dioxane; ethanol; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: 1609259-55-3
4-(4,6-dimethylpyrimidin-5-yl)-3-methylphenol

: 1609577-45-8
4-[4-(4,6-dimethylpyrimidin-5-yl)-3-methylphenoxy]-3-methylfuro[3,2-c]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / dimethyl sulfoxide / 3 h / 120 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane; water; ethanol / 14 h / 120 °C / Inert atmosphere; Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; caesium carbonate; In 1,4-dioxane; ethanol; water; dimethyl sulfoxide;