Technology Process of C25H29NO6
There total 4 articles about C25H29NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C18H21NO5; 4-methoxyphenylboronic acid;
With
chlorobis(cyclooctene)rhodium(I) dimer; (R)-N-cinnamyl-2-methylpropane-2-sulfinamide;
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
Inert atmosphere;
With
potassium hydroxide;
In
tetrahydrofuran; water;
at 20 ℃;
for 12h;
enantioselective reaction;
Inert atmosphere;
DOI:10.1039/c2ob26316e
DOI:10.1039/c2ob26316e
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dmap / dichloromethane / 3 h / 20 °C
2.1: (R)-N-cinnamyl-2-methylpropane-2-sulfinamide; chlorobis(cyclooctene)rhodium(I) dimer / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
2.2: 12 h / 20 °C / Inert atmosphere
With
dmap; chlorobis(cyclooctene)rhodium(I) dimer; (R)-N-cinnamyl-2-methylpropane-2-sulfinamide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/c2ob26316e
DOI:10.1039/c2ob26316e
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrahydrofuran / 0.5 h
2.1: dmap / dichloromethane / 3 h / 20 °C
3.1: (R)-N-cinnamyl-2-methylpropane-2-sulfinamide; chlorobis(cyclooctene)rhodium(I) dimer / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
3.2: 12 h / 20 °C / Inert atmosphere
With
dmap; chlorobis(cyclooctene)rhodium(I) dimer; (R)-N-cinnamyl-2-methylpropane-2-sulfinamide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/c2ob26316e
DOI:10.1039/c2ob26316e
