3-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-methyl-benzaldehyde

Base Information

Chemical Name:3-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-methyl-benzaldehyde
CAS No.:1026964-22-6
Molecular Formula:C₁₅H₂₂O₄S
Molecular Weight:298.403
Hs Code.:

Synonyms:3-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-methyl-benzaldehyde

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Chemical Property of 3-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-methyl-benzaldehyde

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Technology Process of 3-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-methyl-benzaldehyde

There total 5 articles about 3-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-methyl-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 339354-90-4
3-({2-[2-(2-methoxyethoxy)ethoxy]ethyl}sulfanyl)-2-methylbenzyl alcohol

: 1026964-22-6
3-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-methyl-benzaldehyde

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 0.75h;
DOI:10.1021/jm0208673

Reference yield:

: 52130-17-3
3-amino-2-methylbenzoic acid

: 1026964-22-6
3-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-methyl-benzaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaNO₂; H⁺

1.2: potassium ethyl xanthogenate; aq. Na₂CO₃ / pH 8

1.3: 14.66 g / aq. NaOH / 20 h / Heating

2.1: 93 percent / H₂SO₄ / 48 h / Heating

3.1: 96 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

4.1: 51 percent / Et₃N / acetonitrile / 72 h / 20 °C

5.1: MnO₂ / CH₂Cl₂ / 0.75 h / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; sulfuric acid; hydrogen cation; triethylamine; sodium nitrite; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jm0208673

Reference yield:

: 339354-89-1
2-methyl-3-sulfanylbenzyl alcohol

: 1026964-22-6
3-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-methyl-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / Et₃N / acetonitrile / 72 h / 20 °C

2: MnO₂ / CH₂Cl₂ / 0.75 h / 20 °C

With manganese(IV) oxide; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/jm0208673