2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)benzyl(4-acetoxy)benzoate

Base Information

• Chemical Name: 2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)benzyl(4-acetoxy)benzoate
• CAS No.: 1590385-31-1
• Molecular Formula: C₃₀H₃₂O₁₄
• Molecular Weight: 616.576

Synonyms:2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)benzyl(4-acetoxy)benzoate

Chemical Property of 2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)benzyl(4-acetoxy)benzoate

Chemical Property:

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Technology Process of 2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)benzyl(4-acetoxy)benzoate

There total 1 articles about 2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)benzyl(4-acetoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranozyloxy)benzyl alcohol (122186-40-7) + 4-acetyloxy-benzoic acid (2345-34-8) → 2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)benzyl(4-acetoxy)benzoate (1590385-31-1)

Guidance literature:

With pyridine; In chloroform; at 20 ℃; for 24h;

DOI:10.1016/j.carres.2014.02.014

Reference yield: 80.0%

2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)benzyl(4-acetoxy)benzoate (1590385-31-1) → 2-(β-D-glucopyranosyloxy)benzyl (4-hydroxy)benzoate (1590385-40-2)

Guidance literature:

With hydrogenchloride; In ethanol; chloroform; water; at 30 ℃;

DOI:10.1016/j.carres.2014.02.014

upstream raw materials:

2-(2,3,4,6-tetra-O-acetyl-β-_D-glucopyranozyloxy)benzyl alcohol

4-acetyloxy-benzoic acid

Downstream raw materials:

2-(β-D-glucopyranosyloxy)benzyl (4-hydroxy)benzoate

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