N-benzyloxycarbonyl-N-tert-butyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine methyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-N-tert-butyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine methyl ester
CAS No.:588719-15-7
Molecular Formula:C₃₅H₄₃N₅O₇
Molecular Weight:645.756
Hs Code.:

Synonyms:N-benzyloxycarbonyl-N-tert-butyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine methyl ester

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Chemical Property of N-benzyloxycarbonyl-N-tert-butyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine methyl ester

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Technology Process of N-benzyloxycarbonyl-N-tert-butyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine methyl ester

There total 3 articles about N-benzyloxycarbonyl-N-tert-butyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 588719-10-2
N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine methyl ester

: 588719-15-7
N-benzyloxycarbonyl-N-tert-butyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine methyl ester

: N-benzyloxycarbonyl-N,ω-bis(tert-butyloxycarbonyl)-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine methyl ester

Guidance literature:: With dmap; In acetonitrile; at 20 ℃; for 72h;
DOI:10.1039/b212470j

Reference yield:

: 20691-84-3
m-methyl red

: 588719-15-7
N-benzyloxycarbonyl-N-tert-butyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / DCC; HOBt / dimethylformamide

2: 35 percent / DMAP / acetonitrile / 72 h / 20 °C

With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b212470j

Reference yield:

: 26348-68-5
N-(benzyloxycarbonyl)lysine methyl ester hydrochloride

: 588719-15-7
N-benzyloxycarbonyl-N-tert-butyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / DCC; HOBt / dimethylformamide

2: 35 percent / DMAP / acetonitrile / 72 h / 20 °C

With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b212470j