4-methoxybenzyl 5-cyano-5-deoxy-2,3-O-isopropylidene-α-D-lyxofuranoside

Base Information

Chemical Name:4-methoxybenzyl 5-cyano-5-deoxy-2,3-O-isopropylidene-α-D-lyxofuranoside
CAS No.:1382059-93-9
Molecular Formula:C₁₇H₂₁NO₅
Molecular Weight:319.357
Hs Code.:

Synonyms:4-methoxybenzyl 5-cyano-5-deoxy-2,3-O-isopropylidene-α-D-lyxofuranoside

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Chemical Property of 4-methoxybenzyl 5-cyano-5-deoxy-2,3-O-isopropylidene-α-D-lyxofuranoside

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Technology Process of 4-methoxybenzyl 5-cyano-5-deoxy-2,3-O-isopropylidene-α-D-lyxofuranoside

There total 4 articles about 4-methoxybenzyl 5-cyano-5-deoxy-2,3-O-isopropylidene-α-D-lyxofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1382059-92-8
4-methoxybenzyl 2,3-O-isopropylidene-α-D-lyxofuranoside

: 1382059-93-9
4-methoxybenzyl 5-cyano-5-deoxy-2,3-O-isopropylidene-α-D-lyxofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

2: N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

With pyridine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol3013638

Reference yield:

: 164665-83-2
2,3-O-isopropylidene-1-O-p-methoxybenzyl-α-D-mannofuranoside

: 1382059-93-9
4-methoxybenzyl 5-cyano-5-deoxy-2,3-O-isopropylidene-α-D-lyxofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: sodium periodate / water; acetone / 2 h / 20 °C

2: sodium tetrahydroborate / methanol / 2 h / 0 °C

3: pyridine / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

4: N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; sodium periodate; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ol3013638

Reference yield:

: 333717-22-9
4-methoxybenzyl 2,3-O-isopropylidene-α-D-lyxo-pentodialdo-1,4-furanoside

: 1382059-93-9
4-methoxybenzyl 5-cyano-5-deoxy-2,3-O-isopropylidene-α-D-lyxofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 2 h / 0 °C

2: pyridine / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

3: N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol3013638