benzyl 5-(3,4-dichlorophenyl)pentan-2-ylcarbamate

Base Information

Chemical Name:benzyl 5-(3,4-dichlorophenyl)pentan-2-ylcarbamate
CAS No.:1429204-87-4
Molecular Formula:C₁₉H₂₁Cl₂NO₂
Molecular Weight:366.287
Hs Code.:

Synonyms:benzyl 5-(3,4-dichlorophenyl)pentan-2-ylcarbamate

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Chemical Property of benzyl 5-(3,4-dichlorophenyl)pentan-2-ylcarbamate

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Technology Process of benzyl 5-(3,4-dichlorophenyl)pentan-2-ylcarbamate

There total 7 articles about benzyl 5-(3,4-dichlorophenyl)pentan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1339931-04-2
5-(3,4-dichlorophenyl)pentan-2-amine

: 501-53-1,94274-21-2
benzyl chloroformate

: 1429204-87-4
benzyl 5-(3,4-dichlorophenyl)pentan-2-ylcarbamate

Guidance literature:: With sodium carbonate; In tetrahydrofuran; at 20 ℃; for 18h;

Reference yield:

: 39960-05-9
3-(3 ,4-dichlorophenyl)propan-1-ol

: 1429204-87-4
benzyl 5-(3,4-dichlorophenyl)pentan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 6 steps

1.1: methane sulfonyl chloride / pyridine / 3 h / 20 °C

1.2: 72 h / 0 - 20 °C

2.1: sodium hydroxide / ethanol / 3 h / 20 °C / Reflux

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 3 h / 20 °C

4.1: tetrahydrofuran; toluene / 3 h / 0 - 20 °C

5.1: ammonium formate; sodium cyanoborohydride / methanol / 0.33 h / 20 °C

5.2: 2 h / 20 °C

6.1: sodium carbonate / tetrahydrofuran / 20 °C

With methane sulfonyl chloride; ammonium formate; sodium cyanoborohydride; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; toluene;

Reference yield:

: 25157-66-8
4-(3,4-dichlorophenyl)butanoic acid

: 1429204-87-4
benzyl 5-(3,4-dichlorophenyl)pentan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 3 h / 20 °C

2.1: tetrahydrofuran; toluene / 3 h / 0 - 20 °C

3.1: ammonium formate; sodium cyanoborohydride / methanol / 0.33 h / 20 °C

3.2: 2 h / 20 °C

4.1: sodium carbonate / tetrahydrofuran / 20 °C

With ammonium formate; sodium cyanoborohydride; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;