6-Amino-2-[4-(5,5-dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-benzo[de]isoquinoline-1,3-dione

Base Information

• Chemical Name: 6-Amino-2-[4-(5,5-dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-benzo[de]isoquinoline-1,3-dione
• CAS No.: 106834-35-9
• Molecular Formula: C₂₃H₂₁N₂O₆P
• Molecular Weight: 452.403

Synonyms:6-Amino-2-[4-(5,5-dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-benzo[de]isoquinoline-1,3-dione

Chemical Property of 6-Amino-2-[4-(5,5-dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-benzo[de]isoquinoline-1,3-dione

Chemical Property:

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Technology Process of 6-Amino-2-[4-(5,5-dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-benzo[de]isoquinoline-1,3-dione

There total 3 articles about 6-Amino-2-[4-(5,5-dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-benzo[de]isoquinoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.5%

2-[4-(5,5-Dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-6-nitro-benzo[de]isoquinoline-1,3-dione (106834-32-6) → 6-Amino-2-[4-(5,5-dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-benzo[de]isoquinoline-1,3-dione (106834-35-9)

Guidance literature:

With hydrazine hydrate; nickel; In ethanol; for 7h; Heating;

Reference yield:

2,2-dimethyltrimethylene p-nitrophenyl phosphate (1028-00-8) → 6-Amino-2-[4-(5,5-dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-benzo[de]isoquinoline-1,3-dione (106834-35-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 55 percent /

2: 69 percent / acetic acid / 2 h / Heating

3: 53.5 percent / hydrazine hydrate / Raney nickel / ethanol / 7 h / Heating

With ; hydrazine hydrate; nickel; In ethanol; acetic acid;

Reference yield:

p-aminophenyl 2,2-dimethyltrimethylene phosphate (106834-29-1) → 6-Amino-2-[4-(5,5-dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-benzo[de]isoquinoline-1,3-dione (106834-35-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / acetic acid / 2 h / Heating

2: 53.5 percent / hydrazine hydrate / Raney nickel / ethanol / 7 h / Heating

With hydrazine hydrate; nickel; In ethanol; acetic acid;

upstream raw materials:

2-[4-(5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-6-nitro-benzo[de]isoquinoline-1,3-dione

2,2-dimethyltrimethylene p-nitrophenyl phosphate

p-aminophenyl 2,2-dimethyltrimethylene phosphate

Downstream raw materials:

C₄₁H₃₄N₂O₆P₂

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