1,3,4,6-tetra-O-acetyl-2-amino-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranose

Base Information

• Chemical Name: 1,3,4,6-tetra-O-acetyl-2-amino-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranose
• CAS No.: 142981-91-7
• Molecular Formula: C₃₅H₅₃NO₁₁
• Molecular Weight: 663.806

Synonyms:1,3,4,6-tetra-O-acetyl-2-amino-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranose

Chemical Property of 1,3,4,6-tetra-O-acetyl-2-amino-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranose

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Technology Process of 1,3,4,6-tetra-O-acetyl-2-amino-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranose

There total 1 articles about 1,3,4,6-tetra-O-acetyl-2-amino-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H42O5 + tetra-acetyl glucosamine (17460-45-6,23707-23-5,23739-93-7,23743-51-3,26108-75-8,59042-16-9,124516-07-0,124580-56-9) → 1,3,4,6-tetra-O-acetyl-2-amino-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranose (142981-91-7)

Guidance literature:

In dichloromethane; for 16h; Yield given;

DOI:10.1016/0008-6215(94)84290-6

Reference yield: 80.0%

3-allyloxy-1-propanol (6180-67-2) + 1,3,4,6-tetra-O-acetyl-2-amino-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranose (142981-91-7) → 3-allyloxypropyl 3,4,6-tri-O-acetyl-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-β-D-glucopyranoside

Guidance literature:

With calcium sulfate; iron(III) chloride; In dichloromethane; for 24h;

DOI:10.1016/0008-6215(94)84290-6

Reference yield: 65.0%

4-allyloxybutan-1-ol (1471-15-4) + 1,3,4,6-tetra-O-acetyl-2-amino-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranose (142981-91-7) → 4-allyloxybutyl 3,4,6-tri-O-acetyl-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-β-D-glucopyranoside

Guidance literature:

With calcium sulfate; iron(III) chloride; In dichloromethane; for 24h;

DOI:10.1016/0008-6215(94)84290-6

upstream raw materials:

tetra-acetyl glucosamine

Downstream raw materials:

3-methyl>-N-<(R)-3-(benzyloxy)tetradecanoyl>amino>propyl 3,4,6-tri-O-acetyl-2-amino-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranoside

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