phenyl N-phenyl-N-methyldithiocarbamate

Base Information

• Chemical Name: phenyl N-phenyl-N-methyldithiocarbamate
• CAS No.: 21168-04-7
• Molecular Formula: C₁₄H₁₃NS₂
• Molecular Weight: 259.396
• Mol file: 21168-04-7.mol

Synonyms:phenyl N-phenyl-N-methyldithiocarbamate

Chemical Property of phenyl N-phenyl-N-methyldithiocarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl N-phenyl-N-methyldithiocarbamate

There total 5 articles about phenyl N-phenyl-N-methyldithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

iodobenzene (591-50-4) + sodium N-methyl-N-phenyldithiocarbamate (39234-21-4) → phenyl N-phenyl-N-methyldithiocarbamate (21168-04-7)

Guidance literature:

With dimethylaminoacetic acid; copper(l) iodide; In N,N-dimethyl-formamide; at 110 ℃; for 22h;

DOI:10.1016/j.tetlet.2007.03.168

Reference yield:

thiophenol (108-98-5) → phenyl N-phenyl-N-methyldithiocarbamate (21168-04-7)

Guidance literature:

Multi-step reaction with 2 steps

1: chloroform; NaOH; water

2: alcohol

With sodium hydroxide; ethanol; chloroform; water;

Reference yield:

phenyl chlorodithioformate (16911-89-0) + N-methylaniline (100-61-8) → phenyl N-phenyl-N-methyldithiocarbamate (21168-04-7)

Guidance literature:

With ethanol;

upstream raw materials:

phenyl chlorodithioformate

N-methylaniline

N-methyl-N-phenylthiocarbamoyl chloride

iodobenzene

Refernces